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2007 2nd IEEE International Conference on Nano/Micro Engineered and Molecular Systems最新文献

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Surface Profile and Optical Properties of Sb-doped SnO2 Thin Films sb掺杂SnO2薄膜的表面轮廓和光学性质
S. D. Hutagalung, B.Y. Lee
Tin oxide (SnO2) and antimony-doped tin oxide (SnO2:Sb) thin films were deposited on the microscope slide glass substrates by sol-gel dip coating technique. Precursor solution was prepared using tin(IV) chloride pentahydrate, antimony chloride, urea, and hydrochloric acid. The Sb dopant concentration was varied from 1 to 4 mol% to investigate the effect of doping on the optical and surface roughness of the films. AFM image showed that undoped films having a very smooth surface morphology with nanostructure grain size in the range of 37.6 to 56.3 nm. Meanwhile, Sb-doped SnO2 was more roughness if compared to undoped one. The optical properties of the films have been studied from transmission spectra in the ultraviolet-visible wavelength range. Energy gap of Sb-doped SnO2 thin films are in the range of 4.07-4.11 eV, shifted to the lower value with increased doping concentration.
采用溶胶-凝胶浸涂技术在载玻片衬底上制备了氧化锡(SnO2)和掺锑氧化锡(SnO2:Sb)薄膜。用五水氯化锡、氯化锑、尿素和盐酸配制前驱体溶液。Sb掺杂浓度在1 ~ 4 mol%范围内变化,考察掺杂对薄膜光学性能和表面粗糙度的影响。AFM图像显示,未掺杂的薄膜表面形貌非常光滑,纳米结构晶粒尺寸在37.6 ~ 56.3 nm之间。同时,与未掺杂的SnO2相比,sb掺杂的SnO2粗糙度更大。从紫外-可见光透射光谱研究了薄膜的光学性能。sn掺杂SnO2薄膜的能隙在4.07-4.11 eV之间,随着掺杂浓度的增加,能隙逐渐减小。
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引用次数: 3
Photocatalytic Oxidation and Alkylation Processes in Microreactors 微反应器中的光催化氧化和烷基化过程
Y. Matsushita, M. Iwasawa, N. Ohba, S. Kumada, T. Suzuki, T. Ichimura
A microflow reaction system with immobilized a photocatalytic TiO2 layer was developed and the processes of oxidation of aromatic compounds and amine N-alkylation in microspace were examined. The photocatalytic microreactor has a remarkably large surface-to-volume ratio in comparison to conventional batch reactors and these model reactions proceeded very rapidly with considerably large efficiencies. The results suggest the feasibility of a photocatalytic microreaction system on organic reactions.
建立了固定化光催化TiO2微流反应体系,研究了微空间中芳香族化合物的氧化和氨基n -烷基化过程。与传统的间歇式反应器相比,光催化微反应器具有非常大的表面体积比,并且这些模型反应进行得非常快,效率相当高。结果表明光催化微反应体系用于有机反应是可行的。
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引用次数: 1
Nano Self-Assembled Nanoparticle Ion-Sensitive Field-Effect Transistors for Acetylcholine Biosensing 用于乙酰胆碱生物传感的纳米自组装纳米粒子离子敏感场效应晶体管
Yi Liu, A. Erdman, T. Cui
We present an inexpensive way to fabricate high-performance nanoparticle based ion-sensitive field-effect transistors (ISFETs) for the acetylcholine biosensing application. The fabrication is implemented with a low-cost layer-by-layer nano self-assembly and microfabrication techniques. Self-assembled silica nanoparticle thin film and indium oxide nanoparticle thin film work as the gate dielectric and semiconducting channel respectively. The ISFETs operate at a low-voltage range of less than 2 V, and has a high mobility of 43.10 cm2/Vs. Acetylcholine in a concentration as low as 100 nM could be detected with this sensor. The results presented herein suggest a route to inexpensive, high mobility ion-sensitive field-effect transistors for biosensing applications.
我们提出了一种廉价的方法来制造高性能的基于纳米粒子的离子敏感场效应晶体管(isfet),用于乙酰胆碱生物传感应用。制造是通过低成本的层层纳米自组装和微加工技术实现的。自组装二氧化硅纳米颗粒薄膜和氧化铟纳米颗粒薄膜分别作为栅介质和半导体通道。isfet工作在低于2v的低电压范围内,并且具有43.10 cm2/Vs的高迁移率。该传感器可检测浓度低至100 nM的乙酰胆碱。本文提出的结果为生物传感应用提供了一条廉价、高迁移率的场效应晶体管的途径。
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引用次数: 4
Forensic Fingerprint Enhancement using Bioadhesive Chitosan and Gold Nanoparticles 生物胶粘剂壳聚糖和金纳米颗粒的法医指纹增强研究
N. Islam, Kazi F. Ahmed, Abhilash Sugunan, Joydeep Dutta
Detection of latent fingerprints using lipophilic and polycationic polymer chitosan has been explored. The gold nanoparticle deposition on chitosan treated latent fingerprints enhances contrast, making the fingerprint identification possible. Chitosan being the second most abundant natural polymer, this technique can be an inexpensive and efficient method for fingerprint enhancement and its subsequent detection. This simple technique has a potential of immediate application in forensic science.
探讨了用亲脂性和聚阳离子性聚合物壳聚糖检测潜在指纹的方法。金纳米颗粒沉积在壳聚糖处理过的指纹上,增强了指纹的对比度,使指纹识别成为可能。壳聚糖作为储量第二丰富的天然聚合物,是一种廉价、高效的指纹增强及其后续检测方法。这种简单的技术在法医学上有立即应用的潜力。
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引用次数: 9
Fabrication of Three Dimensional X-ray Mask using MEMS Technology 利用MEMS技术制作三维x射线掩模
H. Mekaru, T. Takano, K. Awazu, M. Takahashi, R. Maeda
The authors fabricated silicon microstructures with inclined sidewalls on the SOI wafer by using tapered-RIE technique. Then, this wafer was processed to an X-ray mask that made the silicon structure an X-ray absorber. The inclined angle of the sidewall of silicon X-ray absorbers has been changed from 60 to 71 degrees by adjusting the pressure of the mixed gas in the process chamber of the ICP-RIE system. The thickness distribution of the X-ray absorber is different according to the difference of the inclined angle of the X-ray absorber. As a result, the transmission intensity of X-rays is locally changed, and the energy distribution of X-rays irradiated on a resist can be controlled. The authors experimented on the X-ray lithography using this X-ray gray mask and the beamline BL-4 in the synchrotron radiation facility TERAS of AIST. As a result, we succeeded in fabrication of three-dimensional PMMA microstructures by only one X-ray exposure without scanning and rotating the X-ray exposure stage.
采用锥形rie技术在SOI晶圆上制备了具有倾斜侧壁的硅微结构。然后,将该晶圆加工成x射线掩膜,使硅结构成为x射线吸收剂。通过调整ICP-RIE系统过程室中混合气体的压力,使硅x射线吸收器侧壁的倾斜角由60度改变为71度。x射线吸收体的厚度分布随x射线吸收体倾斜角度的不同而不同。这样可以局部改变x射线的透射强度,从而控制x射线照射在阻片上的能量分布。作者在AIST的同步辐射设备TERAS上用该x射线灰色掩模和光束线BL-4进行了x射线光刻实验。因此,我们成功地制造了三维PMMA微结构,只需一次x射线曝光,而无需扫描和旋转x射线曝光阶段。
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引用次数: 0
Anchor Loss Reduction in Resonant MEMS using MESA Structures 利用MESA结构降低谐振MEMS中的锚损
M. Pandey, R. Reichenbach, A. Zehnder, A. Lal, H. Craighead
The quality factor of an oscillator is inversely proportional to the damping and is a measure of the width of its amplitude vs. forcing frequency response. For sensing and signal processing applications of microelectromechanical systems (MEMS) oscillators, the quality factor (henceforth called Q) affects the sensitivity and performance of such devices. As MEMS vibrates (resonates) some of its vibrational energy is transmitted to the substrate upon which the MEMS is fabricated. A large component of this energy is carried away as surface acoustic waves (SAW). We demonstrate a design that improves the Q of resonant MEMS oscillators by up to 4times by reflecting surface wave energy back to the MEMS. Wave reflection occurs at trenches fabricated in a circle around the MEMS. The trench creates a "mesa" that provides partial mechanical isolation to the MEMS. The loss of energy due to SAW increases almost exponentially with frequency, with a corresponding decrease in Q. Hence the demonstrated design would become even more useful with the increasing need for higher frequency resonators. The mesa structure presented here is a simple idea which can be easily integrated into existing fabrication procedures and can be used for commercial purposes.
振荡器的质量系数与阻尼成反比,是对其振幅宽度与强迫频率响应的度量。对于微机电系统(MEMS)振荡器的传感和信号处理应用,质量因子(以下称为Q)影响着此类器件的灵敏度和性能。当MEMS振动(共振)时,它的一些振动能量被传递到制造MEMS的衬底上。这种能量的很大一部分作为表面声波(SAW)被带走。我们展示了一种设计,通过将表面波能量反射回MEMS,将谐振MEMS振荡器的Q提高了4倍。波反射发生在MEMS周围的圆形沟槽中。该沟槽创建了一个“台面”,为MEMS提供部分机械隔离。由于SAW的能量损失几乎随频率呈指数增长,相应的q值也会降低。因此,随着对高频谐振器需求的增加,所演示的设计将变得更加有用。这里展示的平台结构是一个简单的想法,可以很容易地集成到现有的制造过程中,并可用于商业目的。
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引用次数: 2
Development of AFM Based on Nano Positioning Stage 基于纳米定位台的AFM的发展
N. Jiao, Yuechao Wang, N. Xi, Z. Dong
A single PZT (piezoelectric) tube is generally used in atomic force microscope (AFM) as its scanner. But due to the kinematic coupling of the single tube during its bending motion, there usually exist two kinds of structure errors: vertical cross coupling error and scanning size error which affect the precision of nano observation and manipulation. In this paper, a new AFM with nano positioning stage as its scanner is developed. The stage has three PZT actuators and can move in three directions with high precision without kinematic coupling, thus the two structure errors are eliminated effectively in the new AFM. Some development results are presented and the experimental results validate the performance of the AFM.
在原子力显微镜(AFM)中,通常使用单个压电管作为扫描器件。但由于单管在弯曲运动过程中存在运动耦合,通常存在两种结构误差:垂直交叉耦合误差和扫描尺寸误差,影响纳米观测和操作的精度。本文研制了一种以纳米定位台为扫描器的新型原子力显微镜。该平台采用三个压电陶瓷作动器,无需运动耦合即可实现高精度的三方向运动,有效地消除了两种结构误差。给出了一些开发结果,实验结果验证了AFM的性能。
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引用次数: 0
A Microfluidic Device for Capture of Single Cells and Impedance Measurement 一种用于单细胞捕获和阻抗测量的微流体装置
Min-Haw Wang, Min-Feng Kao, Haw-Juin Liu, Wai-Hong Kan, Y. Hsu, L. Jang
A microfluidic device for capture of single cells and impedance measurement is presented. The device consists of a PDMS channel with three micro pillars and a glass substrate with electrodes. The experiments demonstrated that the HeLa cell (human cervical epithelioid carcinoma) was successfully captured by the micro pillars and its impedance was measured by impedance spectroscopy. The range of operation voltage is from 0.1 V to 1.5 V and the scan frequency is from 1 kHz to 100 kHz. According to experimental results, the HeLa cell is capacitive and its electrical model can be simplified to the parallel connection with one resistor and one capacitor. This developed technique for cell impedance analysis possesses advantages of physical capture, low cost, and easy of fabrication and measurement.
介绍了一种用于单细胞捕获和阻抗测量的微流控装置。该装置由带有三个微柱的PDMS通道和带有电极的玻璃基板组成。实验表明,微柱成功捕获了人宫颈上皮样癌HeLa细胞,并通过阻抗谱测量了HeLa细胞的阻抗。工作电压范围为0.1 V ~ 1.5 V,扫描频率范围为1khz ~ 100khz。实验结果表明,HeLa电池具有电容性,其电学模型可简化为一个电阻和一个电容并联。该方法具有物理捕获、成本低、易于制作和测量等优点。
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引用次数: 4
High Performance Ethanol Sensor for Control Drunken Driving Based on Flame-made ZnO Nanoparticles 基于火焰法制备ZnO纳米颗粒的醉酒驾驶控制乙醇传感器
C. Liewhiran, A. Camenzind, A. Teleki, S. Pratsinis, S. Phanichphant
ZnO nanoparticles were produced by FSP using zinc naphthenate as a precursor dissolved in toluene/acetonitrile (80/20 vol%). The phase and crystallite size were analyzed by X-ray diffraction (XRD), and the specific surface area (SSA) of the nanoparticles was measured by nitrogen adsorption (BET analysis). The ZnO particle size and morphologies was further investigated by transmission electron microscopy (TEM) revealing spheroidal, hexagonal, and rod-like morphologies. The crystallite sizes of ZnO spheroidal and hexagonal particles were in the range of 10-20 nm. ZnO nanorods were found to be ranging from 10-20 nm in width and 20-50 nm in length. Sensing films were produced by mixing the particles into an organic paste composed of terpineol and ethyl cellulose as a vehicle binder. The paste was doctor-bladed onto Al2O3 substrates interdigitated with Au electrodes. The morphology of the sensing films was analyzed by scanning electron microscopy (SEM). The gas sensing of ethanol (25-250 ppm) was studied at 400 degC in dry air. The oxidation of ethanol on the surface of the semiconductor was confirmed by mass spectroscopy (MS). Thick (5 mum) ZnO films showed high sensitivity and fast response times (within seconds). The sensitivity increased and the response time decreased with increasing ethanol concentration. These concentrations (25-250 ppm) were corresponded to be almost in the same range with detection limit of concentration for human breath analyzer. These sensor can be performed an ethanol sensing device that could be employed for control of drunken driving.
以环烷酸锌为前驱体,溶解在甲苯/乙腈(80/20 vol%)中,采用FSP法制备了氧化锌纳米颗粒。用x射线衍射(XRD)分析了纳米颗粒的物相和晶粒尺寸,用氮吸附(BET)分析了纳米颗粒的比表面积(SSA)。通过透射电子显微镜(TEM)进一步研究了ZnO的粒径和形貌,揭示了球体、六边形和棒状形貌。氧化锌的晶粒尺寸在10 ~ 20 nm之间。ZnO纳米棒的宽度为10 ~ 20nm,长度为20 ~ 50nm。传感膜是通过将颗粒混合到由松油醇和乙基纤维素作为载体粘合剂组成的有机糊状物中来生产的。将该浆料均匀地涂在与Au电极交叉的Al2O3衬底上。利用扫描电子显微镜(SEM)对传感膜的形貌进行了分析。在400℃的干燥空气中研究了乙醇(25-250 ppm)的气敏。质谱分析证实了乙醇在半导体表面的氧化作用。厚(5 μ m) ZnO薄膜具有高灵敏度和快速响应时间(秒级)。随着乙醇浓度的增加,灵敏度增加,响应时间缩短。这些浓度(25 ~ 250 ppm)与人体呼吸分析仪的浓度检测限基本一致。这些传感器可以执行乙醇传感装置,可用于酒后驾驶的控制。
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引用次数: 6
Self-Assembled Heterogeneous Integrated Fluorescence Detection System 自组装异质集成荧光检测系统
S.S. Kim, E. Saeedi, D. Meldrum, B. Parviz
We present the current progress towards a fully integrated fluorescence detection system constructed via self-assembly of independently microfabricated excitation sources and photosensors onto a common template. The system template contains specifically shaped binding sites for micron-scale components and electrical interconnects. The self-assembly process allows for using materials such as plastic or glass for constructing the template that are incompatible with conventional microfabrication processes. The excitation sources are AlGaAs light emitting diodes and the photosensors are silicon pn junctions. These microcomponents are independently microfabricated and released from their respective substrates to yield a powder-like collection. The microcomponents are introduced over the template in a heated fluidic slurry and allowed to self-assemble onto the complementary-shaped binding sites. The self-assembly process is driven by capillary forces resultant from low melting point alloy coated on the electrical contact pads, fluidic forces, shape matching, and gravity. The final system offers a 3 times 3 array of individually addressable complete fluorescence detection units.
我们介绍了一种完全集成的荧光检测系统的最新进展,该系统是通过将独立的微制造激发源和光传感器自组装到一个共同的模板上构建的。系统模板包含用于微米级组件和电气互连的特殊形状的结合位点。自组装工艺允许使用塑料或玻璃等材料来构建与传统微加工工艺不兼容的模板。激发源为AlGaAs发光二极管,光传感器为硅pn结。这些微组分被独立地微加工,并从各自的底物中释放出来,以产生粉末状的集合。微组件在加热的流体浆液中引入模板,并允许自组装到互补形状的结合位点上。自组装过程由涂覆在电接触垫上的低熔点合金、流体力、形状匹配和重力产生的毛细力驱动。最后的系统提供了一个3 × 3阵列的单独可寻址的完整荧光检测单元。
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引用次数: 7
期刊
2007 2nd IEEE International Conference on Nano/Micro Engineered and Molecular Systems
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