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2007 2nd IEEE International Conference on Nano/Micro Engineered and Molecular Systems最新文献

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The Effect of Substrate Temperature on Structure and Optical Properties of Copper (II) Phthalocyanine (CuPc) Thin Films Prepared by Organic Evaporation 衬底温度对有机蒸发法制备酞菁铜(CuPc)薄膜结构和光学性能的影响
S. Kamoldilok, B. Tunhoo, S. Sumriddetchkajorn, J. Nukeaw
The influence of substrate temperature controls on copper (II) phthalocyanine (CuPc) organic thin films onto glass substrate by organic evaporation system has been examined by X-ray diffraction (XRD), field emission scanning electron microscope (FE-SEM) and UV-VIS spectrophotometer. The two control methods are an on-off switching temperature control and a phase temperature control. The various substrate temperatures were controlled at 27, 80, 100, 120 and 150 degC, respectively. The thickness of all thin films is 30 nm. The XRD results from both methods show strongly peaks in orientation of [200] plane as alpha-phase monoclinic structure. By an on-off switching controlled temperature, the intensity of XRD peaks is increased with increasing substrate temperature. While intensity of XRD results from a phase controlled temperature shows increasing from 27 to 100 degC but decreasing from 120 to 150 degC. The CuPc grown at 150 degC exhibits nanorod-like structure obtained from an on-off switching temperature control and fiber-like structures obtained from a phase temperature controls. The optical absorptions of CuPc thin films of both methods determined from UV-VIS spectrophotometer show two strong peaks at 330 nm and 620 nm, denoted the B-band and Q-band, respectively.
采用x射线衍射仪(XRD)、场发射扫描电镜(FE-SEM)和紫外可见分光光度计(UV-VIS)研究了衬底温度控制对有机蒸发法制备玻璃衬底上酞菁铜(CuPc)有机薄膜的影响。两种控制方法是开关温度控制和相位温度控制。衬底温度分别控制在27、80、100、120和150℃。所有薄膜的厚度均为30 nm。两种方法的XRD结果均显示[200]平面的取向峰为α相单斜结构。通过开关控制温度,XRD峰的强度随衬底温度的升高而增加。而相控温度下的XRD强度在27 ~ 100℃范围内增大,在120 ~ 150℃范围内减小。在150℃下生长的CuPc显示出通过开关温度控制获得的纳米棒状结构和通过相温度控制获得的纤维状结构。紫外-可见分光光度计测定两种方法的CuPc薄膜的光吸收在330 nm和620 nm处有两个强峰,分别为b波段和q波段。
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引用次数: 1
Development of Optical Fibre Sensors for Online pH Monitoring in Microbioreactors 用于微生物反应器pH在线监测的光纤传感器的研制
Min-Hsien Wu, Junbo Wang, Jr-Lung Lin, Z. Cui, Z. Cui
The development of non-invasive optical fibre sensor array for on-line monitoring of pH in microbioreactors is described. The working principle is based on the optical absorption of phenol red contained in culture medium. Different from other devices of the similar working principle, the proposed device requires less liquid volume (less than 0.8 mul), is non-invasive, and particularly can be configured as an array. The computer simulation and experimental results revealed that the design of oval detection chamber can substantially reduce the response time. Also, the system was proved to be able to detect pH change (pH 6.8-7.8) experienced in normal cell culture.
介绍了用于微生物反应器中pH值在线监测的非侵入式光纤传感器阵列的研制。其工作原理是基于对培养基中所含酚红的光学吸收。与其他类似工作原理的设备不同,该设备所需的液体体积较小(小于0.8 mul),无创性,特别是可以配置为阵列。计算机仿真和实验结果表明,椭圆形检测室的设计可以大大缩短响应时间。此外,该系统被证明能够检测正常细胞培养中pH值的变化(pH值6.8-7.8)。
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引用次数: 1
Study on Space Morphology of Molecular Structure of Tungsten Trioxide Compound Film Surface by AFM 原子力显微镜研究三氧化钨复合膜表面分子结构的空间形貌
Ding Zhong, Hui Yang, Xueheng Yang, Yan Xu, Xianwu Han, Xiaoping Su, Anping Liu, Taiguo Tang, Changshui Chen
In this paper, the molecular structures of tungsten trioxide (WO3) crystal film surfaces are studied by AFM.IPC-208B, and their XRD spectrums are also analyzed. Two types of crystal film are: WO3 sol-gel film adulterated with platinum and WO3 magnetron ion sputtering film adulterated with platinum. The studies on WO3 sol-gel film adulterated with platinum show that it has been cubic crystal after annealing at 460degC, its crystal cell includes a WO6 octahedron in which six oxygen ions locate in the center of six planes of cube and one tungsten ion locates in the center of cube, its lattice parameter is about 0.75 plusmn 0.05 nm, its natural growth surface is (002) plane on which its one cell includes five ions, four oxygen ions locate in the culminations of quadrangle and one tungsten ion locates in the center of quadrangle, and the distance between two adjacent oxygen ions is about 0.55 plusmn 0.05 nm. Meanwhile the studies on WO3 magnetron ion sputtering film adulterated with platinum find that it has also been plate crystal after annealing at 400degC , its crystal cell includes four tetrahedrons, its natural growth surface is (106) plane on which its one cell includes three tungsten ions and seven oxygen ions or two tungsten ions and eight oxygen ions, these ions locate in the culminations of four coterminous quadrangles, and its lattice parameters are about 1.35 plusmn 0.05 nm and 0.35 plusmn 0.05 nm, respectively. The above results on molecular structures of WO3 crystal film surfaces have never been seen in overseas or home reports.
本文采用原子力显微镜研究了三氧化钨(WO3)晶体膜表面的分子结构。对IPC-208B进行了XRD分析。掺杂铂的WO3溶胶-凝胶膜和掺杂铂的WO3磁控离子溅射膜两种类型的晶体膜。对掺杂铂的WO3溶胶-凝胶膜的研究表明,在460℃退火后,WO3溶胶-凝胶膜已成立方晶体,其晶胞包括一个WO6八面体,其中6个氧离子位于立方体的6个平面中心,1个钨离子位于立方体的中心,其晶格参数约为0.75 plusmn 0.05 nm,其自然生长面为(002)平面,其中一个晶胞包含5个离子。四个氧离子位于四边形的顶点,一个钨离子位于四边形的中心,两个相邻氧离子之间的距离约为0.55±0.05 nm。同时,对掺杂铂的WO3磁控离子溅射膜的研究发现,在400℃退火后,其晶胞包括4个四面体,其自然生长面为(106)面,其中一个晶胞包含3个钨离子和7个氧离子或2个钨离子和8个氧离子,这些离子位于4个共端四边形的顶点。其晶格参数分别约为1.35 plusmn 0.05 nm和0.35 plusmn 0.05 nm。上述关于WO3晶体膜表面分子结构的结果,国内外均未见报道。
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引用次数: 0
Novel Carbon Nanotube Deposition System for Fabricating Nano Devices 制备纳米器件的新型碳纳米管沉积系统
K. Lai, N. Xi
Carbon nanotubes (CNTs) are found to be promising material for nanoelectronics due to its ultra small size and unique properties. It provides the possibility of miniaturizing conventional electronic devices, and therefore, people have focused on exploring its applications in nanoelectronics, such as replacing the conventional transistors, resisters and sensors, etc. In order to study its properties and use them as novel devices, methods to manipulate such nano sized particles on micro electrodes have to be developed. Since the size of CNTs is in nano scale, traditional robotic manipulation and assembly cannot be applied. A novel and effective CNT manipulation method is developed and presented in this paper. An automatic and robotic CNT deposition system is used to manipulate CNT across micro electrodes precisely by dielectrophertic (DEP) force. It is also integrated with micromanipulator, micro pump and micro pipette to deposit CNT dilution in desired positions of micro electrodes. This system can potentially be used to fabricate and manufacture an array of CNT based sensors, resulting in a fast, automatic and feasible method for batch making and assembling nano devices.
碳纳米管以其超小的尺寸和独特的性能被认为是纳米电子学中很有前途的材料。它为传统电子器件的小型化提供了可能,因此人们一直致力于探索其在纳米电子学中的应用,如取代传统的晶体管、电阻和传感器等。为了研究其性质并将其作为新型器件使用,必须开发在微电极上操纵纳米级颗粒的方法。由于碳纳米管的尺寸为纳米级,传统的机器人操作和装配无法应用。本文提出了一种新颖有效的碳纳米管操纵方法。一个自动化和机器人碳纳米管沉积系统被用来操纵碳纳米管在微电极上精确地介电(DEP)力。它还集成了微操纵器,微泵和微移液器,以沉积碳纳米管稀释在微电极的所需位置。该系统可以潜在地用于制造一系列基于碳纳米管的传感器,从而为批量制造和组装纳米器件提供了一种快速、自动和可行的方法。
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引用次数: 3
Manipulation of Bioparticles on Electrodeless Dielectrophoretic Chip Based on AC Electrokinetic Control 基于交流电动控制的生物微粒在无极介电芯片上的操作
Hsien-Chang Chang, Chao-Hung Chen, I. Cheng, Chi-Chang Lin
An electrodeless dielectrophoretic (EDEP) chip was designed and applied to separate the micro-particles in different sizes, and the ability of bio-separation of real samples also be examined. The dielectrophoretic (DEP) force can be principally created and controlled by provide a non-uniform electric field that is geometrically constricted by the insulator-patterned chip in combination with an alternative current (AC) electric field at frequency 10 kHz and 500 Vp-p set on the two sides of channel inlet. The EDEP chip was used to separate the E. coli and red blood cells (RBC), which from human whole blood sample, via well control of DEP force. Our results showed the bacteria and RBC can be separated into the higher and lower electric field regions of the EDEP chip in few seconds, respectively. A rapid, useful diagnosis tool, based on the EDEP method could be applied and used in the various fields of the bio-industry technology, the detection and the identification of clinical infections.
设计了一种无电极介电泳(EDEP)芯片,用于分离不同粒径的微颗粒,并对实际样品的生物分离能力进行了检验。介电泳(DEP)力主要可以通过提供一个非均匀的电场来产生和控制,该电场由绝缘体图案芯片在几何上收缩,并结合频率为10 kHz和500 Vp-p的交流(AC)电场设置在通道入口两侧。EDEP芯片通过良好的DEP力控制,从人全血样品中分离大肠杆菌和红细胞。结果表明,细菌和红细胞可以在几秒内分别被分离到EDEP芯片的高电场区和低电场区。基于EDEP方法的快速、实用的诊断工具可应用于生物工业技术、临床感染的检测和鉴定等各个领域。
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引用次数: 2
Meniscus Pinned Variable-focus Liquid Lens Based on Electrowetting-on-dielectric 基于介质电润湿的半月板固定变焦液体透镜
Ming Kang, Ruifeng Yue, Jiangang Wu, Fan Ouyang, Litian Liu
A novel configuration of variable-focus liquid lens based on electrowetting-on-dielectric technique is presented, which consists of a glass slide growing a conductive indium tin oxide (ITO) film and a hydrophobic dielectric film, a hollow conical metal ring suspended right above, a gap between the slide and the ring, and the lens liquid (water). By changing the voltage applied to grounded metal ring and the ITO control electrode, both the position and curvature of the liquid meniscus can be reversibly adjusted, thus tuning the focal length of the lens. The experimental results show that at a 40 V power supply, the liquid lens is able to focus on objects from 2.5 centimeters up to infinity away with a good imaging quality.
提出了一种基于介电润湿技术的变焦液体透镜的新结构,该结构由生长导电氧化铟锡(ITO)薄膜和疏水介电膜的玻璃载玻片、悬浮在正上方的空心锥形金属环、载玻片与金属环之间的间隙以及透镜液体(水)组成。通过改变施加在接地金属环和ITO控制电极上的电压,可以可逆地调节液体半月板的位置和曲率,从而调节透镜的焦距。实验结果表明,在40 V的电源下,液体透镜能够聚焦2.5厘米到无限远的物体,并具有良好的成像质量。
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引用次数: 6
Two Dimensions Angular Sensor for Micro/Nano Measurement 用于微/纳米测量的二维角传感器
Qinggang Liu, Yiping Li, Wenbing Zhao, Xiaotang Hu
An optical non-contact and compact two dimensions angular sensor for micro angle measurement and nanometer scale measurement is introduced in the paper. The light beam emits from the angular sensor to the micro target and then is reflected back into the sensor. The angular sensor is designed based on optical differential method which adopts two orthogonal optical inner-reflection critical angle prisms. A microprocessor control unit (MCU) is used to carry out the signals' collection, processing, display, communication and control signal's output via upper computer. The measurement resolution is better than 0.05arcsec when the measurement range is set to be plusmn 600arcsec. Moreover, the sensor has the merits of adjustable resolution/range and can measure two dimensional angular displacements synchronously.
介绍了一种用于微角测量和纳米尺度测量的光学非接触紧凑二维角传感器。光束从角度传感器发射到微目标,然后被反射回传感器。角度传感器是基于光学微分法设计的,采用两个正交的光学内反射临界角棱镜。采用微处理器控制单元(MCU)完成信号的采集、处理、显示、通信和上位机控制信号的输出。当测量范围设置为±600arcsec时,测量分辨率优于0.05arcsec。此外,该传感器具有分辨率/范围可调的优点,可以同步测量二维角位移。
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引用次数: 1
Correct DC Operation in RTD-based Ternary Inverters 基于rtd的三元逆变器的正确直流操作
J. Núñez, J. Quintana, M. Avedillo
Multiple-valued logic (MVL) circuits are one of the most attractive applications of the monostable-to-multistable transition logic (MML), and they are on the basis of advanced circuits for communications. However, a proper design is not inherent to the usual MML circuit topologies. This paper analyses the case of an MML ternary inverter, and determines the relations that circuit representative parameters must verify to obtain a correct behaviour.
多值逻辑(MVL)电路是单稳态到多稳态转换逻辑(MML)最具吸引力的应用之一,是先进通信电路的基础。然而,适当的设计并不是通常的MML电路拓扑所固有的。本文分析了MML三元逆变器的实例,确定了电路代表性参数必须验证的关系,以获得正确的行为。
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引用次数: 5
The Effects of Mechanical Thin-film Properties on the Pyroelectric Signals 机械薄膜性质对热释电信号的影响
C. Wei, C. Hsiao, Yuh-Chung Hu
The ZnO pyroelectric sensors with configuration of partially covered electrode were used to discuss the correlation between its voltage responsivity, morphology and mechanical properties of the thin film. The sensor based on pyroelectric thin film deposited by sputtering with RF power of 120 W was revealed higher voltage responsivity than those of 150 W and 90 W for 10-400 times. Meanwhile, the surface morphology reveals less defects and uniform grain size for the RF power of 120 W as characterized by SEM, which can be a symptom of the high voltage responsivity. On the other hand, the effective elastic modulus and hardness of ZnO film sputtered with RF power of 120 W were significantly (P Lt 0.05) larger than that of 90 W (21%) and (32%), and 150 W about 23% and 37%, respectively. Therefore, the effects of sputtering power on the voltage responsivity of the pyroelectric sensor can be analyzed and interpreted by the SEM morphology and its mechanical properties.
采用部分覆盖电极结构的ZnO热释电传感器,讨论了其电压响应性、薄膜形貌和力学性能之间的关系。在120 W射频功率下溅射制备的热释电薄膜传感器显示出比150 W和90 W高10-400倍的电压响应性。同时,在RF功率为120 W时,表面形貌缺陷较少,晶粒尺寸均匀,这可能是高电压响应性的表现。另一方面,射频功率为120 W时溅射ZnO薄膜的有效弹性模量和硬度分别显著(P < 0.05)大于90 W时的21%和32%,大于150 W时的23%和37%。因此,溅射功率对热释电传感器电压响应性的影响可以通过SEM形貌及其力学性能来分析和解释。
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引用次数: 2
Selective Growth of CNT on Ni/Cu Substrate CNT在Ni/Cu衬底上的选择性生长
T. Phetchakul, N. Chomnawang, S. Cheirsirikul, N. Nakachai, E. Ratanaudomphisut, P. Songsiriritthigul
This paper presents a method for selective growth of CNT films. Specific areas for CNT growing were defined by patterning Ni electrodes on a Cu substrate using lithography process. CNT films were grown on the substrate by HFCVD method at atmospheric pressure using ethanol and hydrogen as sources. The films were examined and confirmed with SEM, Raman and EDX analysis. The authors observed that CNT only grow in selective areas of Ni. None can be grown on Cu background. This finding suggests a novel method of selective growth of CNT using Cu as a masking layer. Preliminary results also show possibility of growing CNT across the gaps between 3D interdigital Ni electrodes fabricated by LIGA technique.
本文提出了一种选择性生长碳纳米管薄膜的方法。碳纳米管生长的特定区域是通过使用光刻工艺在Cu衬底上绘制Ni电极来定义的。在常压下,以乙醇和氢气为源,采用HFCVD法在衬底上生长碳纳米管薄膜。用SEM、Raman和EDX分析对薄膜进行了检测和验证。作者观察到碳纳米管只生长在Ni的选择性区域。没有一个可以在Cu背景下生长。这一发现提出了一种利用Cu作为掩蔽层选择性生长碳纳米管的新方法。初步结果还显示了通过LIGA技术制造的三维数字间镍电极之间的间隙生长碳纳米管的可能性。
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引用次数: 1
期刊
2007 2nd IEEE International Conference on Nano/Micro Engineered and Molecular Systems
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