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Effect of Powdered Swarf on Self-Adhesive Moldings with Machining Center Extracted Bamboo Fiber 加工中心提取的竹纤维粉屑对自粘成型的影响
Pub Date : 2024-02-09 DOI: 10.4028/p-ljj4fo
Kaito Tanaka, Reo Kitazaki, T. Hirogaki, E. Aoyama, H. Nobe
To address global environmental challenges and mitigate bamboo-related ecological damage, this study focuses on the development of self-adhesive molded products utilizing solely bamboo fibers and powder obtained through machining center extraction. However, the mechanical properties of these molded products remain inadequate. This study utilizes Scanning Electron Microscope (SEM) and Fourier transform infrared spectrometer (FTIR) analyses to explore the disparities associated with chip size as raw materials for molded products. Bamboo fiber, characterized by its substantial cellulose content and high strength, is contrasted with bamboo powder, which contains significant amounts of lignin and exhibits potential adhesive properties. Building upon these findings, the powder was added to the conventional fiber alone, with results demonstrating that a predetermined ratio (20%) of the powder yields optimal mechanical properties. Moreover, employing a parameter representing the degree of lignin flow utilized in previous molding studies, the study establishes the optimum molding conditions (PD'=1.031) to maximize tensile strength (37.8 MPa) when incorporating a 20% powder mixture.
为应对全球环境挑战,减轻与竹子有关的生态破坏,本研究重点关注仅利用加工中心提取的竹纤维和竹粉开发自粘性模塑产品。然而,这些成型产品的机械性能仍然不足。本研究利用扫描电子显微镜(SEM)和傅立叶变换红外光谱仪(FTIR)分析,探讨了竹纤维作为模塑产品原材料与竹屑尺寸之间的差异。竹纤维的特点是纤维素含量高、强度大,而竹粉则含有大量木质素,具有潜在的粘合性。在这些研究成果的基础上,将竹粉单独添加到传统纤维中,结果表明竹粉的预定比例(20%)可产生最佳机械性能。此外,该研究还采用了之前成型研究中使用的代表木质素流动程度的参数,确定了最佳成型条件(PD'=1.031),以便在加入 20% 的粉末混合物时最大限度地提高拉伸强度(37.8 兆帕)。
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引用次数: 0
The Role of Cell Collapse Mechanism in Mechanical Performance of Aluminium Foam Fabricated by Melt Processing 细胞塌缩机制在熔融加工制造的铝泡沫机械性能中的作用
Pub Date : 2024-02-09 DOI: 10.4028/p-03cmzt
O. Byakova, S. Gnyloskurenko, Andrey Vlasov, Yan Yevych, N. Semenov, Dmytro Kytranov
The study presents mechanical performance metrics, especially, energy absorption, of aluminium foams fabricated by melt processing with CaCO3 blowing agent without Ca additive. Relatively ductile Al1Mg0.6Si alloy and high strength Al6Zn2.3Mg alloy comprising brittle eutectic domains were employed for the foams manufacture and then examined in conditions of uniaxial quasi-static compression. It was recognized that mechanical response of the foams and energy absorption is radically defined by the mechanism of cell collapse which, in turn, depends on the nature of structural constituents of the cell wall material. In particular, the presence of brittle eutectic domains in the cell wall material of foam based on Al6Zn2.3Mg alloy results in reducing the compressive strength and energy absorption compared to those of foam processed with Al1Mg0.6Si alloy, both deviate markedly from the theoretical predictions. In spite of this experimental verification of foams cell collapse is considered to be strongly required before their engineering application.
本研究介绍了使用 CaCO3 发泡剂(不含 Ca 添加剂)熔融加工制造的铝泡沫的机械性能指标,尤其是能量吸收指标。研究采用了韧性相对较好的 Al1Mg0.6Si 合金和高强度的 Al6Zn2.3Mg 合金(包含脆性共晶畴)来制造泡沫,然后在单轴准静态压缩条件下进行了检验。人们认识到,泡沫的机械响应和能量吸收从根本上取决于细胞塌陷的机理,而细胞塌陷的机理又取决于细胞壁材料结构成分的性质。特别是,与使用 Al1Mg0.6Si 合金加工的泡沫相比,使用 Al6Zn2.3Mg 合金加工的泡沫的细胞壁材料中存在脆性共晶畴,导致抗压强度和能量吸收能力降低,两者都明显偏离理论预测。尽管如此,在工程应用之前,仍需对泡沫的细胞塌陷进行实验验证。
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引用次数: 0
Effect of Individual Alloying Addition on the Microstructure and Creep Behavior of Squeeze Cast AZ91 Magnesium Alloy 单个合金添加物对挤压铸造 AZ91 镁合金微观结构和蠕变行为的影响
Pub Date : 2024-02-09 DOI: 10.4028/p-ix5zle
Hitesh Patil, Abhijit Ghosh, Hemant Borkar
The microstructure of AZ91 (Mg-Al) alloy is comprised of α-Mg and β-Mg17Al12 massive phase. The lower melting point associated with the β-Mg17Al12 phase results in poor creep resistance of the alloy. In the present study, the AZ91 alloy with the addition of calcium (Ca, 1wt%) and cerium (Ce, 1wt%) is cast, and their effect on the microstructure and creep behavior of AZ91 alloy have been investigated. Thermally stable phases such as Al2Ca and Al11Ce3 are introduced in the AZ91 alloy through the addition of Ca and Ce elements. Energy dispersive spectroscopy (EDS) and x-ray diffraction analysis confirmed the presence of these intermetallic phases in the microstructure. Tensile creep tests on the as-cast samples were performed at 175°C temperature under 50 MPa stress. The study shows that the creep resistance of AZ91 alloy is greatly improved with the presence of Al2Ca and Al11Ce3 intermetallic phases because of their better thermal stability than β-Mg17Al12.
AZ91 (镁-铝)合金的微观结构由 α-Mg 和 β-Mg17Al12 块状相组成。β-Mg17Al12相的熔点较低,导致合金的抗蠕变性较差。本研究铸造了添加钙(Ca,1wt%)和铈(Ce,1wt%)的 AZ91 合金,并研究了它们对 AZ91 合金微观结构和蠕变行为的影响。通过添加钙和铈元素,在 AZ91 合金中引入了 Al2Ca 和 Al11Ce3 等热稳定相。能量色散光谱(EDS)和 X 射线衍射分析证实了微观结构中存在这些金属间相。在 175°C 温度和 50 兆帕应力条件下,对铸件样品进行了拉伸蠕变试验。研究结果表明,由于 Al2Ca 和 Al11Ce3 金属间相的热稳定性比 β-Mg17Al12 更好,因此它们的存在大大提高了 AZ91 合金的抗蠕变性。
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引用次数: 0
Effect of Individual Alloying Addition on the Microstructure and Creep Behavior of Squeeze Cast AZ91 Magnesium Alloy 单个合金添加物对挤压铸造 AZ91 镁合金微观结构和蠕变行为的影响
Pub Date : 2024-02-09 DOI: 10.4028/p-ix5zle
Hitesh Patil, Abhijit Ghosh, Hemant Borkar
The microstructure of AZ91 (Mg-Al) alloy is comprised of α-Mg and β-Mg17Al12 massive phase. The lower melting point associated with the β-Mg17Al12 phase results in poor creep resistance of the alloy. In the present study, the AZ91 alloy with the addition of calcium (Ca, 1wt%) and cerium (Ce, 1wt%) is cast, and their effect on the microstructure and creep behavior of AZ91 alloy have been investigated. Thermally stable phases such as Al2Ca and Al11Ce3 are introduced in the AZ91 alloy through the addition of Ca and Ce elements. Energy dispersive spectroscopy (EDS) and x-ray diffraction analysis confirmed the presence of these intermetallic phases in the microstructure. Tensile creep tests on the as-cast samples were performed at 175°C temperature under 50 MPa stress. The study shows that the creep resistance of AZ91 alloy is greatly improved with the presence of Al2Ca and Al11Ce3 intermetallic phases because of their better thermal stability than β-Mg17Al12.
AZ91 (镁-铝)合金的微观结构由 α-Mg 和 β-Mg17Al12 块状相组成。β-Mg17Al12相的熔点较低,导致合金的抗蠕变性较差。本研究铸造了添加钙(Ca,1wt%)和铈(Ce,1wt%)的 AZ91 合金,并研究了它们对 AZ91 合金微观结构和蠕变行为的影响。通过添加钙和铈元素,在 AZ91 合金中引入了 Al2Ca 和 Al11Ce3 等热稳定相。能量色散光谱(EDS)和 X 射线衍射分析证实了微观结构中存在这些金属间相。在 175°C 温度和 50 兆帕应力条件下,对铸件样品进行了拉伸蠕变试验。研究结果表明,由于 Al2Ca 和 Al11Ce3 金属间相的热稳定性比 β-Mg17Al12 更好,因此它们的存在大大提高了 AZ91 合金的抗蠕变性。
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引用次数: 0
Study on the Material Models of the Forming Limit Curves Development for Predicting a Fracture Behavior of AA5754-O in Automotive Parts 用于预测汽车零件中 AA5754-O 断裂行为的成形极限曲线材料模型开发研究
Pub Date : 2024-02-09 DOI: 10.4028/p-qme3i9
Phiraphong Larpprasoetkun, Jidapa Leelaseat, A. Nakwattanaset, Aekkapon Sunanta, S. Suranuntchai
The forming limit curve (FLC) is commonly used to predict the formability behavior of sheet metal after the forming process. In this research, the forming limit curve generated from the Materials Model was applied to analyze and predict the fracture behavior of the fuel tank workpiece, a motorcycle part made of AA5754-O material, using the deep drawing process simulated by the finite element method. The research involved a comparison with actual cracks that occur in the automotive industry after molding. To determine the mechanical properties of the AA5754-O material for use in the forming limit curve, a specimen with a thickness of 1.5 mm was subjected to a tensile strength test, providing the necessary input for the mechanical properties in the forming limit curve based on the Keeler-Beizer equation. The forming limit curve is a correlation graph between major strain and minor strain. When the FLC is created from the Materials Model, it is utilized in conjunction with deep drawing drag simulation in the PAM-STAMP program to predict the fracture point. The accuracy of the mathematically generated FLC in predicting fracture behavior was verified after the deep drawing process. The study found that the FLC based on the Keeler-Beizer equation can accurately predict the cracking behavior of AA5754-O sheet metal, enabling identification of the fracture location during the deep drawing process. One advantage of creating the FLC from the material models is its compatibility with the same material but with different workpiece shapes, allowing its use in conjunction with molding simulations using various programs. This approach saves costs associated with testing to obtain the FLC.
成形极限曲线(FLC)通常用于预测金属板材在成形过程后的可成形性。在这项研究中,应用材料模型生成的成形极限曲线,分析并预测了油箱工件(一种由 AA5754-O 材料制成的摩托车零件)的断裂行为,该工件使用有限元法模拟了深拉工艺。该研究涉及与汽车行业中成型后出现的实际裂纹进行比较。为了确定 AA5754-O 材料的机械性能以用于成形极限曲线,对厚度为 1.5 毫米的试样进行了拉伸强度测试,为基于 Keeler-Beizer 方程的成形极限曲线提供了必要的机械性能输入。成形极限曲线是主要应变和次要应变之间的相关图形。从材料模型创建 FLC 后,它将与 PAM-STAMP 程序中的拉深拖拽模拟相结合,用于预测断裂点。经过拉深过程后,验证了数学生成的 FLC 在预测断裂行为方面的准确性。研究发现,基于 Keeler-Beizer 方程的 FLC 可以准确预测 AA5754-O 板材的开裂行为,从而在拉深过程中确定断裂位置。根据材料模型创建 FLC 的一个优点是,它与相同材料但不同形状的工件兼容,因此可与使用各种程序的成型模拟结合使用。这种方法节省了为获得 FLC 而进行测试的相关成本。
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引用次数: 0
The Iron-Carbon System: Genesis and Morphology of the Eutectic Involving Hyper-Cementite Carbide 铁碳体系:超硬质合金共晶的成因和形态
Pub Date : 2024-02-09 DOI: 10.4028/p-ftv8w5
Vladyslav Mazur
A straightforward technology for the thermal cyclic processing of the Fe-C melt has been developed to induce significant super-cooling before crystallization. Eutectic crystallization of pro-eutectic alloys under substantial super-cooling is demonstrated to be a complex process, comprising several partial crystallization processes and the synchronous dissolution of crystalline phases: austenite and two metastable carbides, Fe3C and Fe7C3. The kinetics of the eutectic transformation L→L+Fe7C3 in its microscopic and thermal (DSC) imaging has been studied. In general, crystallization proceeds according to the scheme L→L+Fe7C3+γ→L+Fe7C3+γ+Fe3C→ Fe7C3+γ+Fe3C. Consequently, plate-like eutectic (Fe7C3+γ) with an austenite matrix and ledeburite (Fe3C+γ) with a cementite matrix are formed. A schematic diagram of the metastable phase equilibria in the Fe-C system is provided. In the conducted experiments, phase transformations occur in two subsystems: Fe-Fe3C (at low supercooling) and Fe-Fe7C3 (a subsystem of metastable equilibria of the second, higher degree of metastability at large supercooling). This is confirmed by the replacement of the carbide phase and different equilibrate concentrations of austenite in metastable equilibrium with each of the carbides.
已开发出一种对铁-碳熔体进行热循环处理的直接技术,可在结晶前引起显著的过冷。在显著过冷条件下,原共晶合金的共晶结晶是一个复杂的过程,包括几个部分结晶过程和结晶相的同步溶解:奥氏体和两种可转移碳化物(Fe3C 和 Fe7C3)。我们对 L→L+Fe7C3 共晶转变的显微和热成像(DSC)动力学进行了研究。一般来说,结晶按照 L→L+Fe7C3+γ→L+Fe7C3+γ+Fe3C→ Fe7C3+γ+Fe3C 的方案进行。因此,形成了以奥氏体为基体的板状共晶(Fe7C3+γ)和以雪明体为基体的斑晶(Fe3C+γ)。图中提供了 Fe-C 体系中蜕变相平衡的示意图。在所进行的实验中,相变发生在两个子系统中:Fe-Fe3C(在低过冷度时)和 Fe-Fe7C3(在高过冷度时的第二种较高蜕变度的蜕变平衡子系统)。碳化物相的置换以及与每种碳化物处于可转移平衡状态的奥氏体的不同平衡浓度证实了这一点。
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引用次数: 0
Features of Microstructural Evolution and Corrosion Behavior of Ti6Al4V Titanium Alloy Fabricated from Elemental Powder Blends 用元素粉末混合物制造的 Ti6Al4V 钛合金的微结构演变和腐蚀行为特征
Pub Date : 2024-02-09 DOI: 10.4028/p-gvgzk5
Serhii Lavrys, Iryna Pohrelyuk, D. Savvakin, Khrystyna Shliakhetka, M. Danyliak
Sintered Ti6Al4V titanium alloys prepared from TiH2/60Al40V powder blends under various technological conditions were studied. The microstructural evolution was investigated by X-ray diffraction, scanning electron microscopy, optical microscopy, and energy dispersive X-ray analysis. The corrosion resistance of sintered titanium alloy was evaluated by the static immersion test in 40 wt.% H2SO4 acid, according to ASTM standard G31-72(2004). Depending on powder metallurgy processing parameters (compaction pressure or sintering temperature), the Ti6Al4V alloy was obtained with various structural features (porosity and structural heterogeneity). It was shown that those structural features of sintered Ti6Al4V titanium alloy are a key microstructural factor that determines their corrosion resistance. For instance, an increase in porosity leads to enhanced corrosion resistance. Based on the current research, the optimal manufacturing regimes of powder metallurgy of Ti6Al4V titanium alloy ensure the achievement of characteristics sufficient for practical use in aggressive conditions of the chemical industry were obtained.
研究了由 TiH2/60Al40V 粉末混合物在不同工艺条件下制备的烧结 Ti6Al4V 钛合金。通过 X 射线衍射、扫描电子显微镜、光学显微镜和能量色散 X 射线分析研究了微观结构的演变。根据 ASTM 标准 G31-72(2004),通过在 40 wt.% H2SO4 酸中的静态浸泡试验评估了烧结钛合金的耐腐蚀性。根据不同的粉末冶金加工参数(压实压力或烧结温度),得到的 Ti6Al4V 合金具有不同的结构特征(孔隙率和结构异质性)。研究表明,烧结 Ti6Al4V 钛合金的这些结构特征是决定其耐腐蚀性的关键微结构因素。例如,孔隙率的增加会导致耐腐蚀性的增强。在当前研究的基础上,获得了 Ti6Al4V 钛合金粉末冶金的最佳制造机制,以确保获得足以在化学工业侵蚀性条件下实际使用的特性。
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引用次数: 0
Investigation of Co-Extrusion Using a Coat Hanger Die with Different Feedblock Cross-Section 使用不同进料块横截面的衣架模具进行共挤的研究
Pub Date : 2024-02-09 DOI: 10.4028/p-rctkv4
Nurdaulet Sharipkhan, Omonini Clifford, Asma Perveen, Di Chuan Zhang, Dong Ming Wei
When using the coat hanger die method for co-extrusion, the biggest challenges often involve maintaining the uniformity of the velocity distribution at the outlet of the die and ensuring the stability of the interface plane. This paper investigates the effect of different cross-section of feed channels connected to the coat hanger die on the velocity and pressure distribution of the flow at different parts of the die. Co-extrusion of LLDPE (Linear Low Density Polyethylene) and HDPE (High Density Polyethylene) polymers is simulated using ANSYS software 2020 R2 for coat hanger die design with rectangular and circular cross-sections inlet geometry; the results are compared for Carreau-Yasuda model to observe the result differences between rectangular and circular coextrusion channels connected to coat hanger die. Our results showed that rectangular cross-section feedblock generated higher values for pressure in comparison with the pressure generated by the circular cross-section feedblock. The maximum velocity generated in the circular feedblock is lower than that generated in the rectangular one, nevertheless there is more uniformity in velocity distribution in circular than rectangular cross-section.
在使用衣架模具法进行共挤时,最大的挑战往往是如何保持模具出口处流速分布的均匀性,以及如何确保界面平面的稳定性。本文研究了与衣架模相连的不同横截面进料通道对模具不同部位流速和压力分布的影响。使用 ANSYS 软件 2020 R2 模拟了 LLDPE(线性低密度聚乙烯)和 HDPE(高密度聚乙烯)聚合物的共挤,设计了矩形和圆形截面进料口几何形状的衣架模;比较了 Carreau-Yasuda 模型的结果,以观察与衣架模相连的矩形和圆形共挤通道的结果差异。结果表明,与圆形截面进料块产生的压力相比,矩形截面进料块产生的压力值更高。圆形进料块产生的最大速度低于矩形进料块,但圆形截面的速度分布比矩形截面更均匀。
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引用次数: 0
Investigation of the Two-Channel Feedblock Zone in Co-Extrusion of Polymers 聚合物共挤过程中双通道进料区的研究
Pub Date : 2024-02-09 DOI: 10.4028/p-rn5jhp
Nurdaulet Sharipkhan, Asma Perveen, Di Chuan Zhang, Dong Ming Wei
A process when different materials are combined to produce a product with multiple layers is called co-extrusion. During this process, polymers are melted in separate machines and then extrudate from different die channels. Once these channels converge, the polymers meet and flow through a single channel. The surface where the two fluids face is called “interface”. It is crucial to maintain the interface's uniformity and stability in order to achieve the desired multi-layered structure. Most of the issues in co-extrusion are related to issues that can be classified into two categories such as polymer encapsulation/interfacial distortion and die swell. To solve these problems, designers focus on improving the interface's stability. This paper examines effects of cross-section modification of the two-channel feedblock on the interface location and velocity and pressure distributions of the flow. The ANSYS software was used to simulate the co-extrusion of polymers, LLDPE and HDPE, in two-channel feedblock with rectangular, circular, and straight slot cross-sections. The results show that sharp corners increase the thickness of dead zones, while rounding them decreases the thickness. Additionally, stadium-shaped (or straight-slot) cross-section channels can move the flow with a higher maximum velocity and thinner boundary layer combining the results of rectangular and circular feedblocks.
将不同材料组合在一起生产多层产品的工艺称为共挤工艺。在这一工艺中,聚合物在不同的机器中熔化,然后从不同的模槽中挤出。一旦这些通道汇合,聚合物就会相遇并流经一个通道。两种流体面对的表面称为 "界面"。为了获得理想的多层结构,保持界面的均匀性和稳定性至关重要。共挤过程中的大部分问题都与聚合物封装/界面变形和模具膨胀等问题有关,可分为两类。为了解决这些问题,设计人员将重点放在提高界面的稳定性上。本文研究了双通道进料块的横截面修改对界面位置以及流动速度和压力分布的影响。使用 ANSYS 软件模拟了聚合物(LLDPE 和 HDPE)在具有矩形、圆形和直槽横截面的双通道喂料块中的共挤过程。结果表明,尖角会增加死区的厚度,而圆角会减少死区的厚度。此外,与矩形和圆形给料块的结果相比,体育场形(或直槽形)横截面通道能以更高的最大速度和更薄的边界层流动。
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引用次数: 0
Consideration of Moisture Factor during Material Selection in Plastic Product Design 塑料产品设计选材时考虑水分因素
Pub Date : 2024-02-09 DOI: 10.4028/p-gmih5f
Burak Kukcu, B. Daşdemir
This research paper aims to investigate the significance of considering the humidity factor during material selection in plastic product design. Humidity is a crucial environmental parameter that can profoundly influence the properties and performance of plastic materials. To ensure the long-term performance and dependability of plastic products, it is essential to comprehend and take into consideration the impacts of moisture on plastics. Humidity plays a fundamental role in the degradation and functional changes of plastic materials. Moisture absorption can lead to reduced mechanical strength and accelerated degradation processes. The selection of appropriate materials that can withstand humid conditions becomes paramount in product design. For this reason it is important to evaluate the moisture absorption properties of plastic materials. Different polymers exhibit varying degrees of moisture diffusion rates that directly affect their performance in humid environments. Evaluation of moisture measurement results allows designers to make informed decisions during material selection. For this reason, we designed an experiment to investigate which material retains less moisture. In our research, we determined 2 different experimental groups. The first of these groups (type A) was kept under normal conditions by adding glass fiber additive at different rates to the PA66 material, and each product with 3 different additives was tested for moisture for 10 days and the results were recorded. In the second experimental group, type B, the products produced with the same material and additives at the same rate were kept in water for 24 hours, then they were removed from the water and moisture tests were performed. It is aimed to make material selection by interpreting the test results and thus to facilitate the making of designs suitable for use.
本研究论文旨在探讨在塑料产品设计中选择材料时考虑湿度因素的意义。湿度是一个重要的环境参数,会对塑料材料的特性和性能产生深远影响。为了确保塑料产品的长期性能和可靠性,理解和考虑湿度对塑料的影响至关重要。湿度对塑料材料的降解和功能变化起着至关重要的作用。吸湿会导致机械强度降低,加速降解过程。在产品设计中,选择能够承受潮湿条件的适当材料至关重要。因此,评估塑料材料的吸湿性能非常重要。不同的聚合物具有不同程度的湿气扩散率,这直接影响了它们在潮湿环境中的性能。通过评估湿度测量结果,设计人员可以在选择材料时做出明智的决定。为此,我们设计了一个实验来研究哪种材料的保湿性更低。在研究中,我们确定了两个不同的实验组。其中第一组(A 组)通过在 PA66 材料中添加不同比例的玻璃纤维添加剂,使其保持在正常条件下,并对每种添加了 3 种不同添加剂的产品进行为期 10 天的湿度测试,并记录结果。在第二组实验,即 B 型实验中,使用相同材料和添加剂以相同比例生产的产品在水中保持 24 小时,然后将其从水中取出并进行湿度测试。这样做的目的是通过解释试验结果来选择材料,从而便于做出适合使用的设计。
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引用次数: 0
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Key Engineering Materials
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