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CHALCOLITHIC/EARLY BRONZE AGE AND ADDITIONAL MAGDALENIAN RADIOCARBON DATES FOR EL MIRÓN CAVE (RAMALES DE LA VICTORIA, CANTABRIA, SPAIN). DATE LIST VII 埃尔米隆洞穴(西班牙坎塔布里亚拉马莱斯德拉维克托利亚)的旧石器时代/青铜时代早期和马 格达伦时代的其他放射性碳年代。日期清单 VII
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2024-01-22 DOI: 10.1017/rdc.2023.123
Manuel R González Morales, Borja González-Rabanal, Igor Gutiérrez-Zugasti, David Cuenca-Solana, Lawrence G Straus

There are now 101 radiocarbon dates from the long Paleolithic and post-Paleolithic culture-stratigraphic sequence in El Mirón Cave, Cantabrian Spain. Here we report on two dates on bone from two different humans whose remains were found in disturbed surface sediments in the cave vestibule rear and that confirm the existence of burials in addition to previously reported residential occupations in the vestibule front pertaining to the Chalcolithic and early Bronze Age periods (ca. 5500–3500 cal BP). In another attempt to resolve problems of stratigraphic incoherence of dates from the early Magdalenian periods in the vestibule rear, six new assays on faunal remains from Levels 119, 117, 114, 108, and 106 were run at Queen’s University in Belfast. There continue to be date inversions in the Lower Magdalenian range of levels that may be explained by a combination of intensive anthropic and rodent activity, major rock fall, slope wash and gravity-caused object movements, as well as possible problems in following some thin levels during excavations over a large area and across many years of work in the cave vestibule interior, particularly in the absence of any layers that are culturally sterile or even poor. Nonetheless, the coherent age of the Initial Magdalenian is fully confirmed by a new date from Level 21 in the vestibule front at ca. 22,000–20,500 cal BP), as is the general age range of the Lower Magdalenian (ca. 20,500–18,000 cal BP).

在西班牙坎塔布里亚埃尔米龙洞的旧石器时代和后旧石器时代文化地层序列中,目前已有 101 个放射性碳年代。在此,我们报告了在洞穴前庭后部受扰动的地表沉积物中发现的两个不同人类遗骸骨骼上的两个日期,这两个日期证实了前庭前部除了以前报告过的与旧石器时代和青铜时代早期(约 5500-3500 cal BP)有关的居住地之外,还存在墓葬。为了解决前庭后部马格达莱纳早期地层年代不一致的问题,贝尔法斯特皇后大学对 119、117、114、108 和 106 层的动物遗骸进行了六次新的化验。下马格达莱纳期的层位范围仍然存在日期倒置现象,其原因可能是密集的人类活动和啮齿动物活动、大面积的岩石崩落、斜坡冲刷和重力引起的物体移动,以及在洞穴前庭内部大面积和多年的发掘过程中跟踪一些薄层时可能遇到的问题,尤其是在没有任何文化上不成熟甚至贫乏的层位的情况下。尽管如此,前庭前方第 21 层的一个新的年代(约公元前 22,000-20,500 年)完全证实了马格达勒纪初期的一致年代,下马格达勒纪的一般年代范围(约公元前 20,500-18,000 年)也是如此。
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引用次数: 0
OPTICALLY STIMULATED LUMINESCENCE (OSL) MORTAR DATING INTER-COMPARISON STUDY. THE SECOND ROUND OF MODIS, MORTAR DATING INTER-COMPARISON STUDY 光激发发光(OSL)灰泥年代相互比较研究。第二轮莫迪斯、灰泥定年相互比较研究
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2024-01-18 DOI: 10.1017/rdc.2023.124
Petra Urbanová, Laura Panzeri, Jorge Sanjurjo-Sánchez, Marco Martini, Francesco Maspero, Pierre Guibert, Anna Galli
After an intercomparison age experiment carried out in the framework of the first MODIS (MOrtar Dating Inter-comparison Study) project, the results showed general agreement both between optically stimulated luminescence (OSL) dating laboratories and with radiocarbon (14C) dating results. As the needs for the selection of samples convenient for an inter-comparison are not the same between 14C and OSL, for the second running, it has been decided to choose two different sample sets, one to share between the radiocarbon labs and one for the OSL dating ones. The results obtained by applying different experimental protocols (multigrain and single grain techniques) and different statistical models (weighted mean, central age mode, average dose model, minimum age model and exponential exposure dose) are discussed in this work.
在第一个 MODIS(MOrtar Dating Inter-comparison Study)项目框架内进行的年代比对实验结果表明,光激发发光(OSL)年代测定实验室之间以及与放射性碳(14C)年代测定结果之间的比对结果基本一致。由于 14C 定年和 OSL 定年在选择便于相互比对的样品方面的要求不尽相同,因此在第二次比对中,决定选择两套不同的样品,一套供放射性碳实验室共享,另一套供 OSL 定年实验室使用。这项工作讨论了采用不同的实验方案(多颗粒和单颗粒技术)和不同的统计模型(加权平均值、中心年龄模式、平均剂量模型、最小年龄模型和指数暴露剂量)所得到的结果。
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引用次数: 0
A VIEW FROM THE COUNTRYSIDE: RADIOCARBON CHRONOLOGY FOR ZAOLINHETAN OF THE PRE-ZHOU CULTURE IN EARLY DYNASTIC CHINA 从乡村看世界中国早期先周文化枣林河滩的放射性碳年代学
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2024-01-18 DOI: 10.1017/rdc.2023.121
Xiaojian Li, Wei Liu, Yongxiang Xu, Haifeng Dou, A Mark Pollard, Ruiliang Liu
The conquest of the Shang Dynasty at Anyang around 1046 BCE by the Zhou is one of the major events for not only Chinese Bronze Age but also early interaction between the pastoralist groups from the Eurasian Steppes and agriculture ones in the Central Plains of China. It is well-known from historical texts that the pre-Zhou people lived in the ancient Bin region (豳), the exact location of which is unclear, but most likely in the Jing River valley. At some point the leader Gugong Danfu (古公亶父) moved from Bin to the capital Qi (Zhouyuan), which preceded the Zhou invasion of Anyang. We have produced a new high resolution radiocarbon chronology for Zaolinhetan, a small settlement in the pre-Zhou heartland. This shows not only an exceptionally long chronological span for the site, but also a different phasing compared to the traditional pottery typology, which raises new questions regarding the regional variation of pottery typologies. Intriguingly, the analysis also reveals a rapid abandonment of Zaolinhetan around 1100 BCE, at the same time many larger sites, such as Zhouyuan, which later became the capital of the Western Zhou dynasty, were significantly expanding. We argue that the drastic decline of Zaolinhetan as revealed by the substantial number of radiocarbon dates and probably also the movement of pre-Zhou political center from Bin to Qin, was part of bigger picture that involved a range of social and environmental factors.
周人于公元前 1046 年左右在安阳征服商朝,这不仅是中国青铜时代的重大事件之一,也是欧亚草原游牧民族与中国中原农耕民族早期交往的重大事件之一。史书记载,先周人生活在古豳地区,具体位置不详,但很可能在泾河流域。古公亶父从豳迁都齐国(周原),比周朝入侵安阳更早。我们为先周中心地带的一个小聚落枣林河滩制作了新的高分辨率放射性碳年代学。这不仅表明该遗址的年代跨度特别长,而且与传统的陶器类型学相比,其分期也有所不同,这就提出了有关陶器类型学区域差异的新问题。耐人寻味的是,分析还揭示出枣林河滩在公元前 1100 年左右被迅速废弃,与此同时,许多大型遗址,如后来成为西周王朝都城的周原,都在显著扩张。我们认为,大量放射性碳年代所揭示的枣林河滩的急剧衰落,以及先周政治中心从豳到秦的迁移,都是涉及一系列社会和环境因素的大事件的一部分。
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引用次数: 0
AMS 14C DATING AND STABLE ISOTOPE ANALYSIS ON AN 8-KYR OYSTER SHELL FROM TAIPEI BASIN: SEA LEVEL AND SST CHANGES 对台北盆地 8 年生牡蛎贝壳的氨基比林 14c 测定和稳定同位素分析:海平面和地下水位的变化
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2024-01-17 DOI: 10.1017/rdc.2023.117
Hong-Chun Li, Horng-Sheng Mii, Tsung-Kwei Liu, Wen-Shan Chen, Su-Chen Kang, Chun-Yen Chou, Satabdi Misra, Tzu-Tsen Shen, Meixun Zhao

Seven accelerator mass spectrometry radiocarbon (AMS 14C) dates (7260±106∼7607±95 BP averaged 7444±103 BP) on a giant oyster shell, collected from an ancient shore of the Taipei Basin, are similar to the LSC (liquid scintillation counting) 14C age (7260±46 BP) of a grass sample inside the shell. The calibrated 14C ages of the C. gigas by Marine20 are 7490±240∼7805±230 cal BP (average 7660±96 cal BP), generally agreed with the calibrated LSC 14C ages of the grass and the oyster shell. Combined with other 14C ages of shoreline samples in the Taipei Basin, it is evident that sea level rose from 8600 to 7600 cal BP and reached a stand higher than modern sea level. During this marine transgression, the sedimentation rate along the shoreline was very high because 14C dating was not able to detect age differences for 4–5 m thick sediment sequences. Sixty-nine analyses of δ18O and δ13C from the oldest part of the shell exhibit clear seasonal cycles, with a 4-year period of growth in the 5.5-cm section. According to the δ18O values, the ancient oyster grew in a warmer-than-present shoreline environment, suggesting that the current absence of the giant oyster in Taiwan is not due to warming conditions.

在台北盆地古海岸采集的巨牡蛎壳上的 7 个加速器质谱放射性碳(AMS 14C)年代(7260±106∼7607±95 BP,平均 7444±103 BP)与壳内草样的 LSC(液体闪烁计数)14C 年代(7260±46 BP)相近。经 Marine20 标定的千头鳕 14C 年龄为 7490±240∼7805±230 卡 BP(平均 7660±96 卡 BP),与草样和牡蛎壳的 LSC 14C 年龄基本一致。结合台北盆地其他海岸线样本的 14C 年龄,可以看出海平面从公元前 8600 年上升到公元前 7600 年,并达到高于现代海平面的高度。由于 14C 测定法无法检测到 4-5 米厚的沉积序列的年龄差异,因此在这一海洋跃迁过程中,海岸线的沉积速率非常高。贝壳最古老部分的 69 项 δ18O 和 δ13C 分析显示出明显的季节性周期,5.5 厘米部分的生长期为 4 年。根据δ18O值,古牡蛎的生长环境比现在的海岸线环境温暖,这表明目前台湾没有巨牡蛎并不是因为气候变暖。
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引用次数: 0
COMPREHENSIVE UPDATE OF MARINE RESERVOIR VALUES FOR NEW ZEALAND COASTAL WATERS TO INFORM COASTAL HAZARD RESEARCH 全面更新新西兰沿海水域海洋储量值,为沿海灾害研究提供信息
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2024-01-17 DOI: 10.1017/rdc.2023.120
Kate J Clark, Jocelyn C Turnbull, Bruce A Marshall, Taylor W A Ferrick, Jamie D Howarth

Marine radiocarbon (14C) ages are an important geochronology tool for the understanding of past earthquakes and tsunamis that have impacted the coastline of New Zealand. To advance this field of research, we need an improved understanding of the radiocarbon marine reservoir correction for coastal waters of New Zealand. Here we report 170 new ΔR20 (1900–1950) measurements from around New Zealand made on pre-1950 marine shells and mollusks killed by the 1931 Napier earthquake. The influence of feeding method, living depth and environmental preference on ΔR is evaluated and we find no influence from these factors except for samples living at or around the high tide mark on rocky open coastlines, which tend to have anomalously low ΔR values. We examine how ΔR varies spatially around the New Zealand coastline and identify continuous stretches of coastline with statistically similar ΔR values. We recommend subdividing the New Zealand coast into four regions with different marine reservoir corrections: A: south and western South Island, ΔR20 –113 ± 33 yr, B: Cook Strait and western North Island, ΔR20 –171 ± 29 yr, C: northeastern North Island, ΔR20 –143 ± 18 yr, D: eastern North Island and eastern South Island, ΔR20 –70 ± 39 yr.

海洋放射性碳(14C)年龄是了解过去影响新西兰海岸线的地震和海啸的重要地质年代工具。为了推进这一领域的研究,我们需要进一步了解新西兰沿海水域的放射性碳海洋储层校正。在此,我们报告了 170 项新的ΔR20(1900-1950 年)测量值,这些测量值来自新西兰周边地区,是对 1950 年前在 1931 年纳皮尔地震中丧生的海洋贝壳和软体动物进行的测量。我们评估了觅食方式、生活深度和环境偏好对 ΔR 的影响,发现除了生活在开阔的岩石海岸线高潮位或高潮位附近的样本外,这些因素对 ΔR 的影响不大,因为这些样本的 ΔR 值往往异常低。我们研究了 ΔR 在新西兰海岸线周围的空间变化情况,并确定了在统计上具有相似 ΔR 值的连续海岸线。我们建议将新西兰海岸细分为四个区域,采用不同的海洋储层校正方法:A:南岛南部和西部,ΔR20 -113 ± 33 年;B:库克海峡和北岛西部,ΔR20 -171 ± 29 年;C:北岛东北部,ΔR20 -143 ± 18 年;D:北岛东部和南岛东部,ΔR20 -70 ± 39 年。
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引用次数: 0
DEVELOPMENT OF A 14C PROTOCOL AT THE LMC14 FOR THE DATING OF CULTURAL HERITAGE MATERIALS: HISTORICAL MORTARS. PARTICIPATION IN THE MODIS INTERNATIONAL INTERCOMPARISON CAMPAIGN 在 LMC14 制定一项 14C 规程,用于确定文化遗产材料的年代:历史性迫击炮。参与莫迪斯国际相互比较活动
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2024-01-11 DOI: 10.1017/rdc.2023.118
Christophe Moreau, Jean-Pascal Dumoulin, Maguy Jaber, Ingrid Caffy, Emmanuelle Delqué-Količ, Cédric Goulas, Stéphane Hain, Marion Perron, Valérie Setti, Marc Sieudat, Bruno Thellier, Lucile Beck

The absolute dating of mortar by accelerator mass spectrometry (AMS) has been the subject of renewed interest for several years. International intercomparison campaigns, called MODIS (MOrtar Dating Intercomparison Study), have been carried out. The first MODIS-1 campaign highlighted limitations in mortar dating, due to the similarity between the primary material to be dated (binder) and the contaminant (exogenous CaCO3). Methods have since emerged to overcome this problem and the need for a good preliminary characterization has been proven. The Laboratoire de Mesure du Carbone 14 (LMC14) took part in the second intercomparison campaign, MODIS2, by applying thermal decomposition increments to distinguish the carbonated binder, the organic matter contaminants (late in formation pyrogenic carbonate, LDH) and limestone. The LMC14 results on MODIS2 are quite conclusive on “pure” re-carbonated lime mortar binders containing little contaminant geological limestone but show their weaknesses for mortars heavily contaminated in Dolomites, which are difficult to discern from the binder. Recommendations for users of radiocarbon (14C) dating on mortar-based materials are made in the conclusion.

近年来,利用加速器质谱法(AMS)对灰泥进行绝对定年重新引起了人们的兴趣。开展了名为 MODIS(灰泥定年相互比较研究)的国际相互比较活动。第一次 MODIS-1 活动突出了灰泥定年的局限性,这是因为要定年的主要材料(粘结剂)和污染物(外源 CaCO3)之间存在相似性。此后,出现了一些方法来克服这一问题,并证明需要进行良好的初步特征描述。碳14测量实验室(LMC14)参加了第二次比对活动 MODIS2,利用热分解增量来区分碳化粘合剂、有机物污染物(形成后期的热成碳酸盐,LDH)和石灰石。MODIS2 上的 LMC14 结果对 "纯 "再碳化石灰砂浆粘合剂(含少量污染地质石灰岩)非常有说服力,但对受到白云石严重污染的砂浆则显示出其弱点,很难将其与粘合剂区分开来。结论中对砂浆材料的放射性碳(14C)年代测定用户提出了建议。
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引用次数: 0
THE INFLUENCE OF PLANT SPECIES AND PRETREATMENT ON THE 14C AGE OF CAREX-DOMINATED PEAT PLANTS OF A PEAT CORE FROM JINCHUAN MIRE, NE CHINA 植物种类及预处理对中国东北金川沼泽泥炭岩芯中以薹草为主的泥炭植物14C年龄的影响
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2023-12-28 DOI: 10.1017/rdc.2023.112
Satabdi Misra, Sneha Kashyap, Chun-Yen Chou, Tingyi Chang, Hong-Chun Li, Xiaoyan Ning, Jing-Jing Sun, Jie Wang, Meixun Zhao

The comparisons among 126 14C dates of Carex samples including separated leaf and root parts with acid (A)-treatment and acid-base-acid (ABA)-treatment, and 48 published 14C dates of bulk peat plants on a 92-cm core from Jinchuan Mire in NE China, indicate old carbon influence (OCI) on the 14C dates. The OCI varies with plant species, pretreatment and peat depth. In vascular peat plants such as Carex, humin fractions (remains after ABA treatment) and humic acids are representative of the original plant precursor, while fulvic acids are regarded as the secondary mobile product which should be removed for 14C dating. ABA- treatment removes both fulvic acids and humic acids, whereas A-treatment gets rid of only fulvic acids. Carex roots uptake more dissolved CO2 in peat water. Carex leaves may use more CO2 (involving degassing CO2) above the peat surface. By removing humic acids throughout ABA treatment, the OCI may vary differently over depth (time). ABA treatment cannot eliminate the fixed OCI in humin fractions of vascular peat plants, instead, this treatment may enhance OCI by removing humic acid which may represent the true age of the plants. In addition, Bacon model results on this core could not show rapid changes in accumulation rate.

在中国东北金川沼泽采集的 92 厘米泥炭岩芯上,对 126 个薹草样品(包括经酸(A)处理和经酸-碱-酸(ABA)处理的分离叶片和根部)的 14C 年代和 48 个已发表的大块泥炭植物的 14C 年代进行了比较,结果表明老碳对 14C 年代的影响(OCI)。OCI 随植物种类、预处理和泥炭深度的不同而变化。在维管泥炭植物(如薹草)中,腐殖质组分(ABA 处理后的残留物)和腐殖酸是原始植物前体的代表,而富里酸被认为是次要的移动产物,在进行 14C 测定时应去除。经 ABA 处理后,富营养化酸和腐植酸都会被去除,而经 A 处理后,只有富营养化酸会被去除。薹草的根吸收泥炭水中更多的溶解二氧化碳。薹草叶片可能会吸收泥炭表面更多的二氧化碳(包括脱气二氧化碳)。通过在整个 ABA 处理过程中去除腐殖酸,OCI 可能会随深度(时间)的不同而变化。ABA 处理无法消除维管泥炭植物腐殖质部分中固定的 OCI,相反,这种处理可能会通过去除腐殖酸来提高 OCI,而腐殖酸可能代表植物的真实年龄。此外,该岩心的培根模型结果无法显示积累率的快速变化。
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引用次数: 0
LAGOA SALGADA: AN OVERVIEW OF A BRAZILIAN HYPERSALINE LAGOON ENVIRONMENTAL STUDIES OVER THE LAST 5000 YEARS USING RADIOCARBON DATE CORRECTIONS 拉戈阿-萨尔加达:利用放射性碳年代校正对巴西一个高盐度泻湖过去 5000 年的环境研究综述
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2023-12-14 DOI: 10.1017/rdc.2023.83
M I Oliveira, C Carvalho, A Assumpção, K Macario, D Amaral, C F Barbosa, F Oliveira, A Bahniuk, C Vasconcelos, A Cruz, A Blanco

The Lagoa Salgada is located in the Paraíba do Sul river delta plain on the coast of Rio de Janeiro state, Brazil, and is one of the few lagoons in the world that have well-developed recent stromatolites. Lagoa Salgada is a hypersaline lagoon formed in a very complex environmental system subjected to terrestrial and oceanic influences under different sea level regimes and climate variations. In addition, sediment and stromatolites are characterized by unusually positive inorganic δ13C VPDB values. For this reason, it has been the target of several geological and paleoenvironmental studies, which, in their great majority, require a geochronological technique in order to determine the changes in the environment over time. When radiocarbon (14C) dating is used, it is necessary to consider some details as the source of 14C in the environment and perform 14C ages calibration accordingly. In the present paper, a bibliographic survey was carried out in order to review the data treatment and improve the environmental evolution discussion based on accurate calibration. Using the Marine20 curve and an undetermined ΔR, we generated growth and depositional models to establish an overview of the formation of this lagoon.

Lagoa Salgada位于巴西里约热内卢州海岸的Paraíba do Sul河三角洲平原,是世界上为数不多的具有发育良好的近代叠层石的泻湖之一。Salgada Lagoa Salgada是在一个非常复杂的环境系统中形成的一个高盐泻湖,在不同的海平面制度和气候变化下,受到陆地和海洋的影响。此外,沉积物和叠层石具有异常正的无机δ13C VPDB值。由于这个原因,它一直是一些地质和古环境研究的目标,这些研究在大多数情况下都需要地质年代学技术来确定环境随时间的变化。当使用放射性碳(14C)定年时,需要考虑一些细节作为环境中14C的来源,并相应地进行14C年龄校准。本文以文献调查为基础,对数据处理进行综述,以完善基于精确定标的环境演变讨论。利用Marine20曲线和一个未确定的ΔR,我们生成了生长和沉积模型,以建立这个泻湖形成的概述。
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引用次数: 0
A RADIOCARBON-BASED MODEL OF CHANGING BURIAL RITES IN EARLY MEDIEVAL ENGLAND 基于放射性碳足迹的中世纪早期英格兰丧葬仪式变化模型
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2023-12-12 DOI: 10.1017/rdc.2023.110
Emma Brownlee

This paper uses a “dates as data” approach to understand how grave good use and cemetery space changed across the early medieval period in England. A series of composite kernel density estimations were created, based on a dataset of nearly 1100 graves with associated radiocarbon dates, from between the fourth and ninth centuries AD. This modeling revealed a previously unrecognized peak in grave furnishing around 600 AD, which coincides with a peak in isolated burials, and a low point for unfurnished graves and for small cemeteries. It argues that this peak is unrecognized as previous models of chronological change have focused only on graves containing chronologically distinctive artifacts and highlights the importance of radiocarbon dating as a way of avoiding this limitation.

本文采用 "日期即数据 "的方法来了解英格兰中世纪早期坟墓的使用情况和墓地空间的变化。根据公元四世纪至九世纪期间近 1100 座坟墓的数据集以及相关的放射性碳年代,创建了一系列复合核密度估计。该模型显示,在公元 600 年左右出现了一个以前未曾发现的墓葬陈设高峰,这与孤立墓葬的高峰以及未陈设墓葬和小型墓地的低点相吻合。报告认为,由于以往的年代变化模型只关注含有年代独特文物的墓葬,因此这一峰值没有被认识到,并强调了放射性碳年代测定作为避免这一局限性的方法的重要性。
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引用次数: 0
RADIOCARBON STEP-COMBUSTION OXIDATION METHOD AND FTIR ANALYSIS OF TRONDHEIM CaCO3 PRECIPITATES OF ATMOSPHERIC CO2 SAMPLES: FURTHER INVESTIGATIONS AND INSIGHTS 对大气二氧化碳样品的 TRONDHEIM CaCO3 预沉淀物的放射性碳梯级凝聚氧化法和傅立叶分析:进一步的研究和见解
IF 8.3 3区 地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS Pub Date : 2023-12-12 DOI: 10.1017/rdc.2023.106
Guaciara M Santos, Christopher A Leong, Pieter M Grootes, Martin Seiler, Helene Svarva, Marie-Josée Nadeau

Eight atmospheric carbon dioxide samples (as calcium carbonate—CaCO3—precipitates) from Lindesnes site (58ºN, 7ºE), belonging to 1963 and 1980 (four samples from each year) and stored at the National Laboratory for Age Determination (NTNU), have been reevaluated through radiocarbon (14C) analysis. Previous 14C results indicated the presence of a contaminant, which was not removed through different chemical cleansing procedures (e.g., hydrochloric acid—HCl and/or hydrogen peroxide—H2O2). Here, we present a follow up investigation using 14C step-combustion and Fourier-transform infrared spectroscopy (FTIR) analysis. Results from 14C data indicate unsuccessful removal of the contaminant, while further FTIR analysis displayed the presence of moisture. This finding alludes to the possibility that the contaminant is of ambient air-CO2 deeply embedded in CaCO3 powders (within clogged CaCO3 pores and/or bonded to the lattice). Samples were found exposed to air-CO2 and humidity. These conditions may have lasted for years, possibly even decades, leading to the 14C offsets detected here.

通过放射性碳(14C)分析,对林德内斯遗址(北纬 58 度,东经 7 度)1963 年和 1980 年(每年四个样本)储存在国家年龄测定实验室(NTNU)的八个大气二氧化碳样本(碳酸钙-CaCO3-沉淀物)进行了重新评估。之前的 14C 分析结果表明存在污染物,但通过不同的化学净化程序(如盐酸-HCl 和/或过氧化氢-H2O2)也无法去除污染物。在此,我们利用 14C 梯度燃烧和傅立叶变换红外光谱(FTIR)分析进行了后续调查。14C 数据的结果表明,污染物的去除并不成功,而进一步的傅立叶变换红外光谱分析则显示出水分的存在。这一发现表明,污染物可能是深藏在 CaCO3 粉末中的环境空气-CO2(在堵塞的 CaCO3 孔隙中和/或与晶格结合)。发现样品暴露在空气-CO2 和湿度中。这些条件可能已持续数年,甚至数十年,从而导致在此检测到 14C 偏移。
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引用次数: 0
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