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Statistical evaluation of the effect of size and strain rate on particle strength of rockfill materials 粒度和应变率对填石材料颗粒强度影响的统计评估
IF 2.4 3区 工程技术 Pub Date : 2024-04-01 DOI: 10.1007/s10035-024-01417-3
Shihao Yan, Shichun Chi, Yu Guo, Jinwei Wang, Xinjie Zhou

The deformation of rockfill materials is mostly caused by particle breakage and subsequent skeleton adjustment. To investigate the effect of size and strain rate on particle strength under seismic load, a series of single particle crushing tests with different sizes and loading rates were conducted. The results show that the particle strength increases with the loading rate, while the size effect on particle strength gradually weakens. Furthermore, within the framework of the weakest chain theory, the failure probability per unit volume and the spatial location distribution of microcracks are discussed, and a statistical model for quasi-static particle strength is established. The spatial location of microcracks follows a power law distribution, and there is a specific power exponent at different strain rates, so that the compound parameters of the particle volume and failure probability are gathered on a master curve determined by the weakest chain statistics. The strain rate effect reduces the failure probability per unit volume and makes the spatial location distribution of microcracks sparser.

填石材料的变形主要是由颗粒破碎和随后的骨架调整引起的。为研究地震荷载作用下粒径和应变速率对颗粒强度的影响,进行了一系列不同粒径和加载速率的单颗粒破碎试验。结果表明,颗粒强度随加载速率的增加而增加,而尺寸对颗粒强度的影响逐渐减弱。此外,在最弱链理论的框架下,讨论了单位体积的破坏概率和微裂纹的空间位置分布,并建立了准静态颗粒强度的统计模型。微裂纹的空间位置遵循幂律分布,在不同应变速率下存在特定的幂指数,因此颗粒体积和破坏概率的复合参数聚集在由最弱链统计确定的主曲线上。应变速率效应降低了单位体积的失效概率,并使微裂纹的空间位置分布更加稀疏。
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引用次数: 0
Scale-up of dry impregnation processes for porous spherical catalyst particles in a rotating drum: experiments and simulations 旋转滚筒中多孔球形催化剂颗粒干法浸渍工艺的放大:实验与模拟
IF 2.4 3区 工程技术 Pub Date : 2024-03-30 DOI: 10.1007/s10035-024-01416-4
Pengfei Xu, Yangyang Shen, Bryant Avila, Hernán A. Makse, Maria S. Tomassone

Catalyst impregnation is the first step and one of the most crucial steps for preparing industrial catalysts. The process is typically performed in rotating vessels with a spray-nozzle to distribute the liquid onto porous catalyst supports until the pore volume is reached. The inter-particle variability of the impregnated liquid inside the particles significantly affects the activity and selectivity of the resulting catalyst. Current scale-up practices lead to poor fluid distribution and inhomogeneity in the liquid content. The aim of this work is to understand the dynamic behavior of the particles under the spray nozzle, which is essential for desired content uniformity, and to develop a scale-up model for the dry impregnation process. In this work, we considered four dimensionless numbers in the scaling analysis. The scale-up rules require that the dimensionless numbers are kept constant for different scales. Both DEM simulations and matching experiments of dry impregnation inside the porous particles were performed for different vessel sizes. The water content of the particles was compared for different times and locations, and the relative standard deviation is calculated from the axial water content. Simulation and experimental results show that particles achieve similar content uniformity at the end of impregnation, confirming that the scale-up rules are applicable to all vessel sizes. The dimensionless numbers give very good scale-up performance since curves collapse indicating similarity in the processes. In addition, the scale-up method is validated for different particle sizes in simulations.

摘要催化剂浸渍是制备工业催化剂的第一步,也是最关键的步骤之一。该过程通常在旋转容器中进行,用喷嘴将液体喷洒到多孔催化剂载体上,直至达到孔隙率。浸渍在颗粒内的液体在颗粒间的变化会极大地影响催化剂的活性和选择性。目前的放大实践导致液体分布不均和液体含量不均匀。这项工作的目的是了解颗粒在喷嘴下的动态行为,这对实现理想的含量均匀性至关重要,并为干法浸渍工艺开发一个放大模型。在这项工作中,我们在缩放分析中考虑了四个无量纲数。放大规则要求无量纲数在不同尺度下保持不变。我们对不同尺寸的容器进行了多孔颗粒内部干浸渍的 DEM 模拟和匹配实验。比较了不同时间和位置下颗粒的含水量,并根据轴向含水量计算出相对标准偏差。模拟和实验结果表明,颗粒在浸渍结束时达到了相似的含水均匀性,这证实了放大规则适用于所有尺寸的容器。无量纲数具有很好的放大性能,因为曲线塌陷表明过程相似。此外,该放大方法还在不同粒度的模拟中得到了验证。
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引用次数: 0
Investigation on the spreading behaviour of sand powder used in binder jet 3D printing 关于粘合剂喷射三维打印中使用的砂粉扩散行为的研究
IF 2.4 3区 工程技术 Pub Date : 2024-03-29 DOI: 10.1007/s10035-024-01420-8
Yulun Xu, Lanzhou Ge, Wenguang Nan

The spreading behaviour of cohesive sand powder is modelled by Discrete Element Method, and the spreadability and the mechanical jamming are focused. The empty patches and total particle volume of the spread layer are examined, followed by the analysis of the geometry force and jamming structure. The results show that several empty patches with different size and shapes could be observed within the spread layer along the spreading direction even when the gap height increases to 3.0D90. Large particles are more difficult to be spread onto the base due to jamming, although their size is smaller than the gap height. Size segregation of particles occurs before particles entering the gap between the blade and base. There are almost no particles on the smooth base when the gap height is small, due to the full-slip flow of particles. The difference of the spread layer and spreadability between the cases with rough and smooth base is reduced by the increase of the gap height. An interesting correlation between jamming effect and local defects (empty spaces) in the powder layer is identified. The resistance to particle rolling is important for the mechanical jamming reported in this work. The jammed particles with a larger size ratio tend to be more stable.

采用离散元法对粘性砂粉的铺展行为进行建模,并重点研究了铺展性和机械干扰。研究了铺展层的空斑块和总颗粒体积,然后分析了几何力和干扰结构。结果表明,即使间隙高度增加到 3.0D90 时,铺展层内沿铺展方向仍可观察到多个不同大小和形状的空斑块。虽然大颗粒的尺寸小于间隙高度,但由于受到干扰,它们更难被铺展到基底上。在颗粒进入叶片和底座之间的间隙之前,颗粒的尺寸会发生偏析。当间隙高度较小时,由于颗粒的全滑动流动,光滑基底上几乎没有颗粒。随着间隙高度的增加,粗糙底座和光滑底座之间的铺展层和铺展性差异减小。我们发现了粉末层中的堵塞效应和局部缺陷(空隙)之间有趣的相关性。颗粒的滚动阻力对本研究中报告的机械堵塞非常重要。尺寸比越大的颗粒越稳定。
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引用次数: 0
Discrete element study of stresses and deformation on gravity retaining wall under static loading 静力荷载下重力挡土墙应力和变形的离散元素研究
IF 2.4 3区 工程技术 Pub Date : 2024-03-28 DOI: 10.1007/s10035-024-01422-6
Prerna Singh, Tanusree Chakraborty, Puneet Mahajan

The study of gravity retaining wall supporting cohesionless soil is performed using the discrete element software Particle Flow Code (PFC), with emphasis on three-dimensional analysis at the grain scale, covering the transition from the initial state to the active state. The soil particles are represented by spherical balls and the rolling resistance linear contact model is used to include the shape effect. The rigid balls are connected by linear parallel bond contact model with a specified strength and stiffness to replicate the physical characteristics of retaining wall. The domain size is reduced by using high g criteria and scaling laws to enhance computational efficiency. The earth pressure coefficient obtained from the present study is compared with the existing analytical and experimental solutions. It is concluded that widely used Coulomb and Rankine methods underestimate the active earth pressure. The total earth thrust acting on the gravity wall is 67.3 kN/m acting at 0.301H above the wall base. The initial state shows a decrease in average coordination number from 5.0 to 3.3 at wall top indicating the debonding of grains and simultaneous decrease in density. In addition, the force chain distribution, porosity, lateral displacement, and axial displacement are investigated. A correlation between the earth pressure coefficient and lateral displacement is also established. The discrete analysis provided valuable insights into the particle-level mechanisms underlying the overall behavior of the retaining wall, contributing to a better understanding of its continuum response.

Graphical Abstract

使用离散元软件粒子流代码(PFC)对支撑无粘性土的重力挡土墙进行了研究,重点是粒度上的三维分析,包括从初始状态到活动状态的过渡。土壤颗粒由球形球表示,滚动阻力线性接触模型包含了形状效应。刚性球通过具有指定强度和刚度的线性平行结合接触模型进行连接,以复制挡土墙的物理特性。为提高计算效率,采用高 g 准则和缩放定律来减小域尺寸。本研究获得的土压力系数与现有的分析和实验解决方案进行了比较。结论是,广泛使用的库仑法和朗肯法低估了活动土压力。作用于重力墙的总土压力为 67.3 kN/m,位于墙基上方 0.301H 处。初始状态显示,墙顶的平均配位数从 5.0 降至 3.3,表明晶粒脱粘,密度同时降低。此外,还研究了力链分布、孔隙率、横向位移和轴向位移。还建立了土压力系数与侧向位移之间的相关性。离散分析为了解挡土墙整体行为的颗粒级机制提供了宝贵的见解,有助于更好地理解其连续响应。
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引用次数: 0
A study of membrane correction accounting for both curvature and tension in DEM simulations of triaxial tests of sand and ballast with two alternative flexible membrane models 在使用两种可选柔性膜模型对砂和压载物的三轴试验进行 DEM 模拟时,对同时考虑曲率和拉力的膜校正进行研究
IF 2.4 3区 工程技术 Pub Date : 2024-03-25 DOI: 10.1007/s10035-024-01419-1
Mathias Tolomeo, Glenn R. McDowell

In DEM simulations of triaxial tests, modelling a flexible lateral membrane is crucial and challenging. It is essential for the correct application of a uniform lateral pressure and for an accurate measurement of sample volume. Here, we introduce a membrane made of triangular facets, and model it as a continuum; we then compare this approach with a well-established method that uses a layer of bonded spheres. With either method, it is also possible to assess the additional stress applied by the membrane as it deforms, i.e. the difference between the stress applied at the boundary and the actual stress within the sample. It is shown that this difference has two origins: the tension developed in the membrane, as it deforms; and the curvature of the membrane, since this causes a vertical component of the confining pressure which can be significant. These findings may be used to inform and improve the membrane correction commonly used in experiments, where similar effects occur.

Graphic abstract

在三轴试验的 DEM 模拟中,对柔性侧膜进行建模至关重要,也极具挑战性。它对于正确施加均匀侧压力和精确测量样品体积至关重要。在这里,我们引入了一种由三角形切面组成的薄膜,并将其作为连续体建模;然后,我们将这种方法与一种使用粘合球层的成熟方法进行比较。无论采用哪种方法,都可以评估膜在变形时施加的附加应力,即施加在边界上的应力与样品内部实际应力之间的差异。结果表明,这种差异有两个原因:一是膜在变形时产生的张力;二是膜的弧度,因为这会导致可能很大的约束压力垂直分量。这些发现可用于指导和改进实验中常用的膜校正,因为在实验中会出现类似的效应。
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引用次数: 0
Collision time in the inelastic bouncing ball model of granular materials 颗粒材料非弹性弹跳球模型中的碰撞时间
IF 2.4 3区 工程技术 Pub Date : 2024-03-21 DOI: 10.1007/s10035-024-01403-9
Junius André F. Balista, Christian Jay P. Magsigay, Caesar A. Saloma

We modified the inelastic bouncing ball model (IBBM) to account for the role of collision time ({tau }_{c}) in defining the dynamics of vertically vibrated confined granular systems. Although ({tau }_{c}) was surmised to be consequential for dissipative systems, previous studies on the accuracy of IBBM did not formally incorporate ({tau }_{c}) as a dynamical variable of the model, focusing instead on other factors during flight, such as air friction. We utilized the discrete element method (DEM) to study the role of ({tau }_{c}) in the granular dynamics, and to cross-validate the efficacy of our reformulation of IBBM to account for the effect of collisions. When the ({tau }_{c}) value is greater than that of ({t}_{0}), which is the first instance that the container acceleration exceeds the gravitational acceleration (g), the time-of-flight decreases, and the location of the bifurcation point shifts in the bifurcation diagram (time-of-flight versus dimensionless acceleration). We model ({tau }_{c}) as representing the range of uncertainty in the occurrence of ({t}_{0}). Assuming a separation of timescale between the dynamics of the collision between the center-of-mass (CM) of the granular system and the container, and the time-of-flight of the CM itself, we propose a supporting but separate model for the dependence of ({tau }_{c}) on Γ. The time-of-flight duration is determined when ({tau }_{c}) is known in the modified IBBM that now produces bifurcation diagrams which are in closer agreement with the DEM simulation results.

Graphical Abstract

我们修改了非弹性弹跳球模型(IBBM),以考虑碰撞时间(({tau }_{c})在定义垂直振动约束颗粒系统动力学中的作用。尽管人们推测({tau }_{c})对耗散系统有影响,但之前关于IBBM准确性的研究并没有正式将({tau }_{c})作为模型的动态变量,而是将重点放在了飞行过程中的其他因素上,如空气摩擦。我们利用离散元素法(DEM)研究了 ({tau }_{c}) 在颗粒动力学中的作用,并交叉验证了我们重新制定的 IBBM 在考虑碰撞影响方面的有效性。当({tau }_{c})值大于({t}_{0})值时,即容器加速度首次超过重力加速度(g)时,飞行时间减小,分岔点的位置在分岔图(飞行时间与无量纲加速度)中发生移动。我们将 ({tau }_{c}) 建立为代表 ({t}_{0}) 发生的不确定性范围的模型。假定颗粒系统的质量中心(CM)与容器之间的碰撞动力学和CM本身的飞行时间之间的时间尺度是分离的,我们为 ({tau }_{c}) 对 Γ 的依赖性提出了一个支持但独立的模型。当 ({tau }_{c})在修改后的 IBBM 中已知时,飞行时间的持续时间将被确定,现在产生的分岔图与 DEM 仿真结果更加一致。
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引用次数: 0
Ballast crushing probability model considering the influence of particle morphology and size 考虑颗粒形态和大小影响的压载破碎概率模型
IF 2.4 3区 工程技术 Pub Date : 2024-03-20 DOI: 10.1007/s10035-024-01414-6
Rui Gao, Zhiwen Yuan, Qihang Hu, Jing Chen

The non-uniform shape and diverse dimensions exert a substantial influence on the distribution of forces within the ballast, hence affecting its bearing capacity. The objective of this work was to investigate the interrelated impact of particle shape and size on ballast strength, and then construct a prediction model that could estimate the chance of ballast crushing. For these purposes, both three-dimensional scanning and single-particle compression tests were undertaken. The morphology of ballast particles at various scales was comprehensively characterized by computing diverse parameters based on the scanning results. The present study systematically assessed the impact of size, overall shape and roundness on particle crushing behavior and parameters. Then a novel approach was introduced to calculate characteristic strength, taking into account the influence of particle morphology. A ballast crushing probability distribution model was established, which incorporated the Weibull model. The anticipation of ballast crushing probabilities can be achieved within this framework by analyzing particle size and morphology parameters. At last, the actual crushing probabilities were compared to the predicted probabilities for a sample of 50 randomly chosen ballasts. The results revealed that 80% of the particles displayed a deviation of less than 10%, which proved the accuracy of the applied method.

摘要 不均匀的形状和不同的尺寸会对压载物内部的力分布产生重大影响,从而影响其承载能力。这项工作的目的是研究颗粒形状和尺寸对压载强度的相互影响,然后构建一个可估算压载破碎几率的预测模型。为此,我们进行了三维扫描和单颗粒压缩试验。在扫描结果的基础上,通过计算各种参数,全面描述了压载颗粒在不同尺度上的形态特征。本研究系统地评估了粒度、整体形状和圆度对颗粒破碎行为和参数的影响。然后,考虑到颗粒形态的影响,引入了一种计算特征强度的新方法。结合威布尔模型,建立了压载压碎概率分布模型。通过分析颗粒大小和形态参数,可在此框架内预测压载压碎概率。最后,将随机抽取的 50 个压载样本的实际压碎概率与预测概率进行了比较。结果显示,80% 的颗粒偏差小于 10%,这证明了所应用方法的准确性。
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引用次数: 0
Gas flow patterns in a granular fluidized bed 颗粒流化床中的气体流动模式
IF 2.4 3区 工程技术 Pub Date : 2024-03-18 DOI: 10.1007/s10035-024-01415-5
Wilson Barros Jr.

Here we demonstrate the use of magnetic resonance imaging for monitoring a laser-polarized xenon ((^{129})Xe) gas working as a fluidizing phase for a glass bead pack, inside a straight circular tube, simulating a granular gas-fluidized bed. The imaging method enabled encoding spatially resolved velocity and diffusion 2D-axial maps of the gas vertical upflow at variable flow regimes. From these maps one could identify gas flow transitions, hysteresis loops, regions of stagnation, and reversed flow, all of which associated, as well as complementary, to reported flow dynamics probing the particles inside the bed. In particular, we focused on the initial stage of bubbling where quantitative data on gas flow spatial maps and their potential correlation with the granular particles dynamics are scarce.

摘要在这里,我们展示了使用磁共振成像技术来监测激光极化氙((^{129})Xe)气体作为玻璃珠包的流化相在直圆管内的工作情况,模拟颗粒状气体流化床。这种成像方法能够对不同流动状态下气体垂直上升流的空间分辨速度和扩散二维轴向图进行编码。从这些地图中,我们可以识别出气体流动的转变、滞后环、停滞区域和反向流动,所有这些都与探测床内颗粒的流动动力学报告相关,并且是互补的。我们尤其关注起泡的初始阶段,在这一阶段,有关气流空间图及其与颗粒动力学潜在相关性的定量数据非常稀少。
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引用次数: 0
Structural fluctuations in thin cohesive particle layers in powder-based additive manufacturing 基于粉末的增材制造中薄内聚颗粒层的结构波动
IF 2.4 3区 工程技术 Pub Date : 2024-03-13 DOI: 10.1007/s10035-024-01410-w
Sudeshna Roy, Hongyi Xiao, Vasileios Angelidakis, Thorsten Pöschel

Producing dense and homogeneous powder layers with smooth free surface is challenging in additive manufacturing, as interparticle cohesion can strongly affect the powder packing structure and therefore influence the quality of the end product. We use the Discrete Element Method to simulate the spreading process of spherical powders and examine how cohesion influences the characteristics of the packing structure with a focus on the fluctuation of the local morphology. As cohesion increases, the overall packing density decreases, and the free surface roughness increases, which is calculated from digitized surface height distributions. Local structural fluctuations for both quantities are examined through the local packing anisotropy on the particle scale, obtained from Voronoï tessellation. The distributions of these particle-level metrics quantify the increasingly heterogeneous packing structure with clustering and changing surface morphology.

在增材制造中,生产具有光滑自由表面的致密均匀粉末层是一项挑战,因为颗粒间的内聚力会严重影响粉末堆积结构,从而影响最终产品的质量。我们使用离散元素法模拟球形粉末的铺展过程,并研究内聚力如何影响堆积结构的特征,重点关注局部形态的波动。随着内聚力的增加,整体堆积密度降低,自由表面粗糙度增加,这是由数字化表面高度分布计算得出的。通过 Voronoï tessellation 方法获得的颗粒尺度上的局部堆积各向异性,可对这两个量的局部结构波动进行研究。这些颗粒级指标的分布量化了随着聚类和表面形态的变化而日益增多的异质堆积结构。
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引用次数: 0
Microscopic mechanical properties of rockfill materials under different stress paths 不同应力路径下填石材料的微观力学性能
IF 2.4 3区 工程技术 Pub Date : 2024-03-11 DOI: 10.1007/s10035-024-01413-7
Runhan Zhang, Lingkai Zhang, Chong Shi, Yonggang Zhang, Yunchao Cui

The mechanical properties of rockfill materials are not only influenced by microscopic factors such as particle morphology and gradation, but also closely related to different loading stress paths. It is of great significance to study the microscopic mechanical properties of rockfill materials under different stress paths for revealing the macroscopic mechanical properties as well as the microscopic deformation and failure mechanisms of rockfill materials. In this paper, based on the results of triaxial tests, a series of numerical triaxial simulation tests under different stress paths were carried out using the discrete element particle flow method, and the deformation, strength change rules, and fine structure evolution mechanism under three stress paths were explored. The results demonstrated that there were significant differences in the effects of stress paths on the stress–strain and strain-volume change characteristics of the rockfill materials. Stress paths exhibited little effect on the strength characteristics. The anisotropy of strong contact number and strong contact force was the microscopic source of macroscopic strength. The contact situation between the particles was the main microscopic factor affecting the macroscopic deformation. The intrinsic mechanism of macroscopic deformation properties could be revealed by the average coordination number and porosity. The stress path affected the growth rate of the number of bond failures and the total number of failures. The relationship between macroscopic mechanical properties and microstructural evolution under different stress paths was also discussed. The findings can provide meaningful insights into the deformation control and stability analysis of rockfill engineering.

Graphical Abstract

摘要 填石材料的力学性能不仅受颗粒形态、级配等微观因素的影响,还与不同的加载应力路径密切相关。研究不同应力路径下填石材料的微观力学性能,对于揭示填石材料的宏观力学性能以及微观变形和破坏机理具有重要意义。本文在三轴试验结果的基础上,采用离散元粒子流法进行了一系列不同应力路径下的三轴数值模拟试验,探讨了三种应力路径下的变形、强度变化规律和细观结构演化机理。结果表明,应力路径对填石材料应力-应变和应变-体积变化特征的影响存在显著差异。应力路径对强度特征的影响很小。强接触数和强接触力的各向异性是宏观强度的微观来源。颗粒间的接触情况是影响宏观变形的主要微观因素。平均配位数和孔隙率揭示了宏观变形特性的内在机制。应力路径影响了结合失效数和失效总数的增长率。此外,还讨论了不同应力路径下宏观力学性能与微观结构演变之间的关系。研究结果可为填石工程的变形控制和稳定性分析提供有意义的启示。 图表摘要
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引用次数: 0
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Granular Matter
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