Pub Date : 2023-08-01Epub Date: 2023-08-09DOI: 10.1089/3dp.2021.0268
Qiqiang Cao, Yuchao Bai, Zhongpeng Zheng, Jiong Zhang, Jerry Ying Hsi Fuh, Hao Wang
Support removal is one of the thorny issues faced by laser powder bed fusion (LPBF). In particular, the efficient and safe removal of support structures from the thin-walled parts and obtaining high-quality surfaces still remains a challenge owing to their sensitivity to machining. An in-depth understanding of the material response behavior of LPBF thin-walled parts when removing support structures is necessary for overcoming this challenge. The work is divided into two parts: revealing the support removal mechanism and proposing a solution to improve the support machinability. First, the machinability of support structures on thin-walled parts with different thicknesses at different cutting depths was thoroughly investigated. Experimental investigation on cutting force, surface morphology, and deflection were carried out. The results show that cutting forces increase gradually at each cut owing to the tilt and collapse of support structures. The surface morphology is improved as the sample thickness increases but deteriorated as the cutting depth increases. Second, a novel solution of adding resin is proposed to improve the support machinability and good results have been achieved. The z-direction cutting forces for 0.3 and 0.4 mm thickness samples are reduced by 72.6% and 64.6%, respectively, and no deflection of the sample is observed after support removal. Moreover, finite element method simulations are established to further explain the support removal mechanism.
{"title":"Support Removal on Thin-Walled Parts Produced by Laser Powder Bed Fusion.","authors":"Qiqiang Cao, Yuchao Bai, Zhongpeng Zheng, Jiong Zhang, Jerry Ying Hsi Fuh, Hao Wang","doi":"10.1089/3dp.2021.0268","DOIUrl":"10.1089/3dp.2021.0268","url":null,"abstract":"<p><p>Support removal is one of the thorny issues faced by laser powder bed fusion (LPBF). In particular, the efficient and safe removal of support structures from the thin-walled parts and obtaining high-quality surfaces still remains a challenge owing to their sensitivity to machining. An in-depth understanding of the material response behavior of LPBF thin-walled parts when removing support structures is necessary for overcoming this challenge. The work is divided into two parts: revealing the support removal mechanism and proposing a solution to improve the support machinability. First, the machinability of support structures on thin-walled parts with different thicknesses at different cutting depths was thoroughly investigated. Experimental investigation on cutting force, surface morphology, and deflection were carried out. The results show that cutting forces increase gradually at each cut owing to the tilt and collapse of support structures. The surface morphology is improved as the sample thickness increases but deteriorated as the cutting depth increases. Second, a novel solution of adding resin is proposed to improve the support machinability and good results have been achieved. The <i>z</i>-direction cutting forces for 0.3 and 0.4 mm thickness samples are reduced by 72.6% and 64.6%, respectively, and no deflection of the sample is observed after support removal. Moreover, finite element method simulations are established to further explain the support removal mechanism.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"762-775"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10440680/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10115347","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-01Epub Date: 2023-08-09DOI: 10.1089/3dp.2021.0252
Ziqian Wu, Qiling Li, Zhenying Xu
Laser welding quality forecast is highly significant during the laser manufacturing process. However, extracting the dynamic characteristics of the molten pool in the short laser welding process makes predicting of the welding quality in real time difficult. Accordingly, this study proposes a multimodel quality forecast (MMQF) method based on dynamic geometric features of molten pool to forecast the welding quality in real time. For extraction of geometric features of molten pool, an improved fully convolutional neural network is proposed to segment the collected dynamic molten pool images during the entire welding process. In addition, several dynamic geometric features of the molten pool are extracted by using the minimum enclosed rectangle algorithm with an evaluation of the performance by several statistical indexes. With regard to forecasting the welding quality, a nonlinear quadratic kernel logistic regression model is proposed by mapping the linear inseparable features to the high dimensional space. Experimental results show that the MMQF method can make an effective and stable forecast of welding quality. It performs well under small data and can satisfy the requirement of real-time forecast.
{"title":"Laser Welding Multimodel Quality Forecast Method Based on Dynamic Geometric Features of the Molten Pool.","authors":"Ziqian Wu, Qiling Li, Zhenying Xu","doi":"10.1089/3dp.2021.0252","DOIUrl":"10.1089/3dp.2021.0252","url":null,"abstract":"<p><p>Laser welding quality forecast is highly significant during the laser manufacturing process. However, extracting the dynamic characteristics of the molten pool in the short laser welding process makes predicting of the welding quality in real time difficult. Accordingly, this study proposes a multimodel quality forecast (MMQF) method based on dynamic geometric features of molten pool to forecast the welding quality in real time. For extraction of geometric features of molten pool, an improved fully convolutional neural network is proposed to segment the collected dynamic molten pool images during the entire welding process. In addition, several dynamic geometric features of the molten pool are extracted by using the minimum enclosed rectangle algorithm with an evaluation of the performance by several statistical indexes. With regard to forecasting the welding quality, a nonlinear quadratic kernel logistic regression model is proposed by mapping the linear inseparable features to the high dimensional space. Experimental results show that the MMQF method can make an effective and stable forecast of welding quality. It performs well under small data and can satisfy the requirement of real-time forecast.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"723-731"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10440663/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10414380","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-01Epub Date: 2023-08-09DOI: 10.1089/3dp.2021.0265
Navid Alinejadian, Pei Wang, Lauri Kollo, Konda Gokuldoss Prashanth
Commercially pure (cp) molybdenum (Mo) is one of the high-temperature materials of immense potential. It has a body-centered cubic (bcc) structure so it is hard to fabricate using nonequilibrium processes such as the selective laser melting (SLM) without the formation of cracks due to its inherent brittleness. This study deals with the fabrication of dense and near crack-free cp-Mo samples produced by the SLM. The laser scan strategy is adjusted from a single scan to a double scan to reduce the solidification cracks. Samples produced with a laser double scan strategy show a density of ∼99% with a hardness of ∼222 HV.
{"title":"Selective Laser Melting of Commercially Pure Molybdenum by Laser Rescanning.","authors":"Navid Alinejadian, Pei Wang, Lauri Kollo, Konda Gokuldoss Prashanth","doi":"10.1089/3dp.2021.0265","DOIUrl":"10.1089/3dp.2021.0265","url":null,"abstract":"<p><p>Commercially pure (cp) molybdenum (Mo) is one of the high-temperature materials of immense potential. It has a body-centered cubic (bcc) structure so it is hard to fabricate using nonequilibrium processes such as the selective laser melting (SLM) without the formation of cracks due to its inherent brittleness. This study deals with the fabrication of dense and near crack-free cp-Mo samples produced by the SLM. The laser scan strategy is adjusted from a single scan to a double scan to reduce the solidification cracks. Samples produced with a laser double scan strategy show a density of ∼99% with a hardness of ∼222 HV.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"785-791"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10442686/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10069801","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Vladislav Andronov, Libor Beránek, Jan Zajíc, Pavel Šotka, Martin Bock
Metal three-dimensional (3D) printing technology brings several benefits to the field of high-pressure die casting of aluminum, which enhances its development. The associated conformal cooling application is already commonly used where there is a need to improve the quality of castings, increase tool life, or reduce the production cycle. However, will this technology withstand the production of a large part (∼270 × 270 × 200 mm), which will be used directly in the serial production of engine blocks? This article describes a slider with a conformal cooling case study, which was redesigned and manufactured using the laser powder bed fusion (L-PBF) method. After the slider was put into serial production of 1.0 TSI three-cylinder engine blocks, this tool was thoroughly monitored based on the temperature field by comparing the results of a simulation in SW ProCAST with reality, and furthermore examining the influence of the tool on the quality of castings. There was also an evaluation of repairs performed on the tool in the ŠKODA AUTO tool shop and the foundry. These data were compared with a serial tool. Finally, the costs to produce the slider in conventional and 3D-printed variants are compared with an outline of other possible steps for optimizing these costs. The study results show that relatively large parts can be printed and used in serial production even today. It was also confirmed that conformal cooling influenced improving tool life, and the number of repairs in ŠKODA AUTO production also decreased.
{"title":"Case Study of Large Three-Dimensional-Printed Slider with Conformal Cooling for High-Pressure Die Casting.","authors":"Vladislav Andronov, Libor Beránek, Jan Zajíc, Pavel Šotka, Martin Bock","doi":"10.1089/3dp.2022.0225","DOIUrl":"https://doi.org/10.1089/3dp.2022.0225","url":null,"abstract":"<p><p>Metal three-dimensional (3D) printing technology brings several benefits to the field of high-pressure die casting of aluminum, which enhances its development. The associated conformal cooling application is already commonly used where there is a need to improve the quality of castings, increase tool life, or reduce the production cycle. However, will this technology withstand the production of a large part (∼270 × 270 × 200 mm), which will be used directly in the serial production of engine blocks? This article describes a slider with a conformal cooling case study, which was redesigned and manufactured using the laser powder bed fusion (L-PBF) method. After the slider was put into serial production of 1.0 TSI three-cylinder engine blocks, this tool was thoroughly monitored based on the temperature field by comparing the results of a simulation in SW ProCAST with reality, and furthermore examining the influence of the tool on the quality of castings. There was also an evaluation of repairs performed on the tool in the ŠKODA AUTO tool shop and the foundry. These data were compared with a serial tool. Finally, the costs to produce the slider in conventional and 3D-printed variants are compared with an outline of other possible steps for optimizing these costs. The study results show that relatively large parts can be printed and used in serial production even today. It was also confirmed that conformal cooling influenced improving tool life, and the number of repairs in ŠKODA AUTO production also decreased.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"587-608"},"PeriodicalIF":3.1,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://ftp.ncbi.nlm.nih.gov/pub/pmc/oa_pdf/5e/2e/3dp.2022.0225.PMC10440664.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10061430","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-01Epub Date: 2023-08-09DOI: 10.1089/3dp.2021.0161
Lv Du, Wu-Gui Jiang, Gao-Gui Xu, Qing-Hua Qin, Duo-Sheng Li
The finite element (FE) method is used to characterize the thermal gradient, solidification rate, and molten pool sizes of Ti-6Al-4V plates in the process of selective laser melting (SLM). The results are verified by using the computational fluid dynamics (CFD) simulation. The proposed FE model contains a series of toolpath information that is directly converted from a G-code file, including hatch spacing, laser power, layer thickness, dwell time, and scanning speed generated by using Slic3r software from a CAD file. A proposed multi-layer, multi-track FE model is used to investigate the influence of the laser power, scanning speed, and scanning path on the microstructure in the Ti-6Al-4V plate built via SLM. The processing window is also determined based on the proposed FE model. The FE results indicate that, with a decrease in the laser power and an increase in the scanning speed, the morphology of the crystal grains, showing fully columnar crystals, gradually deviates from the fully equiaxed region. The formed grains are dependent on the laser power, scanning speed, and deposition position, but they are not sensitive to the scanning path, and with the deposition from the bottom layer to the top layer, the size of the formed grains is gradually increasing, which shows a good agreement with the experimental results.
采用有限元(FE)方法描述了选择性激光熔化(SLM)过程中 Ti-6Al-4V 板材的热梯度、凝固速率和熔池尺寸。计算流体动力学(CFD)模拟对结果进行了验证。所提出的 FE 模型包含一系列直接从 G 代码文件转换而来的刀具路径信息,包括从 CAD 文件使用 Slic3r 软件生成的舱口间距、激光功率、层厚度、停留时间和扫描速度。利用所提出的多层、多轨道 FE 模型来研究激光功率、扫描速度和扫描路径对通过 SLM 制造的 Ti-6Al-4V 板材微观结构的影响。此外,还根据所提出的 FE 模型确定了加工窗口。有限元分析结果表明,随着激光功率的降低和扫描速度的增加,晶体颗粒的形态逐渐偏离完全等轴区域,呈现出完全柱状晶体。形成的晶粒与激光功率、扫描速度和沉积位置有关,但对扫描路径不敏感,而且随着从底层到顶层的沉积,形成的晶粒尺寸逐渐增大,这与实验结果有很好的一致性。
{"title":"Finite Element Analysis and Computational Fluid Dynamics Verification of Molten Pool Characteristics During Selective Laser Melting of Ti-6Al-4V Plates.","authors":"Lv Du, Wu-Gui Jiang, Gao-Gui Xu, Qing-Hua Qin, Duo-Sheng Li","doi":"10.1089/3dp.2021.0161","DOIUrl":"10.1089/3dp.2021.0161","url":null,"abstract":"<p><p>The finite element (FE) method is used to characterize the thermal gradient, solidification rate, and molten pool sizes of Ti-6Al-4V plates in the process of selective laser melting (SLM). The results are verified by using the computational fluid dynamics (CFD) simulation. The proposed FE model contains a series of toolpath information that is directly converted from a G-code file, including hatch spacing, laser power, layer thickness, dwell time, and scanning speed generated by using Slic3r software from a CAD file. A proposed multi-layer, multi-track FE model is used to investigate the influence of the laser power, scanning speed, and scanning path on the microstructure in the Ti-6Al-4V plate built via SLM. The processing window is also determined based on the proposed FE model. The FE results indicate that, with a decrease in the laser power and an increase in the scanning speed, the morphology of the crystal grains, showing fully columnar crystals, gradually deviates from the fully equiaxed region. The formed grains are dependent on the laser power, scanning speed, and deposition position, but they are not sensitive to the scanning path, and with the deposition from the bottom layer to the top layer, the size of the formed grains is gradually increasing, which shows a good agreement with the experimental results.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"711-722"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10440655/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10114896","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-01Epub Date: 2023-08-09DOI: 10.1089/3dp.2022.0127
Pu Han, Alireza Tofangchi, Sihan Zhang, Julio Jair Izquierdo, Keng Hsu
Fused filament fabrication is one of the most desired thermal plastic additive manufacturing processes because of its ability to fabricate complex objects with high accessibility. However, due to the extrusion track-based direct write process mechanism, parts built using this method exhibit anisotropic mechanical properties. In this work, an in-process laser heating method is introduced to heal interface adhesion between adjacent deposited tracks by increasing the interface temperature to promote polymer reptation and enhance bonding strength of the interface of adjacent tracks. With the use of laser heating induced interface healing, the measured flexural strength between adjacent tracks in the same layer increased and exceeded that of the control sample tested along the track direction. The effect of laser on interface healing was also verified by investigating the load-displacement curve and morphology analysis of the fractured surface.
{"title":"Interface Healing Between Adjacent Tracks in Fused Filament Fabrication Using In-Process Laser Heating.","authors":"Pu Han, Alireza Tofangchi, Sihan Zhang, Julio Jair Izquierdo, Keng Hsu","doi":"10.1089/3dp.2022.0127","DOIUrl":"10.1089/3dp.2022.0127","url":null,"abstract":"<p><p>Fused filament fabrication is one of the most desired thermal plastic additive manufacturing processes because of its ability to fabricate complex objects with high accessibility. However, due to the extrusion track-based direct write process mechanism, parts built using this method exhibit anisotropic mechanical properties. In this work, an in-process laser heating method is introduced to heal interface adhesion between adjacent deposited tracks by increasing the interface temperature to promote polymer reptation and enhance bonding strength of the interface of adjacent tracks. With the use of laser heating induced interface healing, the measured flexural strength between adjacent tracks in the same layer increased and exceeded that of the control sample tested along the track direction. The effect of laser on interface healing was also verified by investigating the load-displacement curve and morphology analysis of the fractured surface.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"808-815"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10440681/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10414378","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-01Epub Date: 2023-08-09DOI: 10.1089/3dp.2021.0133
Chia-Heng Chu, Enerelt Burentugs, Dohwan Lee, Jacob M Owens, Ruxiu Liu, Albert B Frazier, A Fatih Sarioglu
The challenges in reliably removing the sacrificial material from fully enclosed microfluidic channels hinder the use of three-dimensional (3D) printing to create microfluidic devices with intricate geometries. With advances in printer resolution, the etching of sacrificial materials from increasingly smaller channels is poised to be a bottleneck using the existing techniques. In this study, we introduce a microfabrication approach that utilizes centrifugation to effortlessly and efficiently remove the sacrificial materials from 3D-printed microfluidic devices with densely packed microfeatures. We characterize the process by measuring the etch rate under different centrifugal forces and developed a theoretical model to estimate process parameters for a given geometry. The effect of the device layout on the centrifugal etching process is also investigated. We demonstrate the applicability of our approach on devices fabricated using inkjet 3D printing and stereolithography. Finally, the advantages of the introduced approach over commonly used injection-based etching of sacrificial material are experimentally demonstrated in direct comparisons. A robust method to postprocess additively manufactured geometries composed of intricate microfluidic channels can help utilize both the large printing volume and high spatial resolution afforded by 3D printing in creating a variety of devices ranging from scaffolds to large-scale microfluidic assays.
从全封闭微流体通道中可靠地去除牺牲材料是一项挑战,它阻碍了利用三维(3D)打印技术制造具有复杂几何形状的微流体设备。随着打印机分辨率的提高,利用现有技术从越来越小的通道中蚀刻牺牲材料将成为一个瓶颈。在本研究中,我们介绍了一种微制造方法,利用离心分离技术轻松高效地从具有密集微特征的 3D 打印微流控器件中去除牺牲材料。我们通过测量不同离心力下的蚀刻率来描述该工艺,并开发了一个理论模型来估算给定几何形状的工艺参数。我们还研究了器件布局对离心蚀刻过程的影响。我们在使用喷墨 3D 打印和立体光刻技术制造的器件上演示了我们的方法的适用性。最后,通过直接比较,实验证明了所介绍的方法与常用的基于注射的牺牲材料蚀刻方法相比所具有的优势。一种对由错综复杂的微流体通道组成的添加式制造几何形状进行后处理的可靠方法有助于利用三维打印的大打印量和高空间分辨率来制造从支架到大规模微流体检测的各种设备。
{"title":"Centrifugation-Assisted Three-Dimensional Printing of Devices Embedded with Fully Enclosed Microchannels.","authors":"Chia-Heng Chu, Enerelt Burentugs, Dohwan Lee, Jacob M Owens, Ruxiu Liu, Albert B Frazier, A Fatih Sarioglu","doi":"10.1089/3dp.2021.0133","DOIUrl":"10.1089/3dp.2021.0133","url":null,"abstract":"<p><p>The challenges in reliably removing the sacrificial material from fully enclosed microfluidic channels hinder the use of three-dimensional (3D) printing to create microfluidic devices with intricate geometries. With advances in printer resolution, the etching of sacrificial materials from increasingly smaller channels is poised to be a bottleneck using the existing techniques. In this study, we introduce a microfabrication approach that utilizes centrifugation to effortlessly and efficiently remove the sacrificial materials from 3D-printed microfluidic devices with densely packed microfeatures. We characterize the process by measuring the etch rate under different centrifugal forces and developed a theoretical model to estimate process parameters for a given geometry. The effect of the device layout on the centrifugal etching process is also investigated. We demonstrate the applicability of our approach on devices fabricated using inkjet 3D printing and stereolithography. Finally, the advantages of the introduced approach over commonly used injection-based etching of sacrificial material are experimentally demonstrated in direct comparisons. A robust method to postprocess additively manufactured geometries composed of intricate microfluidic channels can help utilize both the large printing volume and high spatial resolution afforded by 3D printing in creating a variety of devices ranging from scaffolds to large-scale microfluidic assays.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"609-618"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10440665/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10059363","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Advances in selective laser melting (SLM) of metals in the past two decades have made metals additive manufacturing more accessible for industrial adoption. Despite printing process improvements, post-processing of SLM components has not improved much, resulting in considerable costs, delay, and design limitations. Building upon recent advances in sensitization-based self-terminating etching processes, this work details a new set iodine-based sensitization and etching chemistries that simplify the post-processing of copper (Cu) alloy components fabricated using SLM. This work demonstrates that iodine can be used to "sensitize" the surface of copper alloy components to form soluble copper iodide salt that can be then dissolved in common solvents, such as acetonitrile. This process removes a predefined amount of material from all interior and exterior surfaces in a self-terminating manner, enabling facile removal of internal and external supports, removal of any trapped powder, and the smoothing of interior and exterior surfaces. We demonstrate this process on GRCop (Cu-chromium-niobium) alloys due to their widespread use by the rocket propulsion industry along with a demonstration in copper (110) for applications in heat exchangers and electromagnetic transmitters/receivers. Our results provide the first systematic study on the effect of iodization temperature and duration on the thickness of the iodide region in GRCop-84 components. Additionally, the surface roughness before and after each iodization-dissolution was also quantified for GRCop-84 and showed 70% reduction in Ra roughness from a high of 10 μm as-printed to a low of 3 μm after four iodization-dissolution cycles.
{"title":"Iodine-Based Sensitization of Copper Alloys to Enable Self-Terminating Etching for Support Removal and Surface Improvements of Additively Manufactured Components.","authors":"Sanaz Yazdanparast, Subbarao Raikar, Meredith Heilig, Owen J Hildreth","doi":"10.1089/3dp.2021.0242","DOIUrl":"10.1089/3dp.2021.0242","url":null,"abstract":"<p><p>Advances in selective laser melting (SLM) of metals in the past two decades have made metals additive manufacturing more accessible for industrial adoption. Despite printing process improvements, post-processing of SLM components has not improved much, resulting in considerable costs, delay, and design limitations. Building upon recent advances in sensitization-based self-terminating etching processes, this work details a new set iodine-based sensitization and etching chemistries that simplify the post-processing of copper (Cu) alloy components fabricated using SLM. This work demonstrates that iodine can be used to \"sensitize\" the surface of copper alloy components to form soluble copper iodide salt that can be then dissolved in common solvents, such as acetonitrile. This process removes a predefined amount of material from all interior and exterior surfaces in a self-terminating manner, enabling facile removal of internal and external supports, removal of any trapped powder, and the smoothing of interior and exterior surfaces. We demonstrate this process on GRCop (Cu-chromium-niobium) alloys due to their widespread use by the rocket propulsion industry along with a demonstration in copper (110) for applications in heat exchangers and electromagnetic transmitters/receivers. Our results provide the first systematic study on the effect of iodization temperature and duration on the thickness of the iodide region in GRCop-84 components. Additionally, the surface roughness before and after each iodization-dissolution was also quantified for GRCop-84 and showed 70% reduction in R<sub>a</sub> roughness from a high of 10 μm as-printed to a low of 3 μm after four iodization-dissolution cycles.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"619-630"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10440683/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10052245","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-01Epub Date: 2023-08-09DOI: 10.1089/3dp.2021.0209
Ratnesh Raj, Amit Rai Dixit
Direct Ink Writing (DIW) opens new possibilities in three-dimensional (3D) printing of carbon-based polymeric ink. This is due to its ability in design flexibility, structural complexity, and environmental sustainability. This area requires exhaustive study because of its wide application in different manufacturing sectors. The present article is related to the variant emerging 3D printing techniques and DIW of carbonaceous materials. Carbon-based materials, extensively used for various applications in 3D printing, possess impressive chemical stability, strength, and flexible nanostructure. Fine printable inks consist predominantly of uniform solutions of carbon materials, such as graphene, graphene oxide (GO), carbon fibers (CFs), carbon nanotubes (CNTs), and solvents. It also contains compatible polymers and suitable additives. This review article elaborately discusses the fundamental requirements of DIW in structuring carbon-doped polymeric inks viz. ink formulation, required ink rheology, extrusion parameters, print fidelity prediction, layer bonding examination, substrate selection, and curing method to achieve fine functional composites. A detailed description of its application in the fields of electronics, medical, and mechanical segments have also been focused in this study.
直接油墨写入(DIW)为碳基聚合物油墨的三维(3D)打印提供了新的可能性。这得益于它在设计灵活性、结构复杂性和环境可持续性方面的能力。由于其在不同制造领域的广泛应用,这一领域需要详尽的研究。本文涉及碳基材料的新型 3D 打印技术和 DIW。碳基材料广泛应用于三维打印的各种领域,具有令人印象深刻的化学稳定性、强度和灵活的纳米结构。精细可打印墨水主要由石墨烯、氧化石墨烯(GO)、碳纤维(CF)、碳纳米管(CNT)等碳材料的均匀溶液和溶剂组成。它还包含兼容的聚合物和合适的添加剂。这篇综述文章详细讨论了 DIW 在掺碳聚合物油墨结构中的基本要求,即油墨配方、所需的油墨流变性、挤出参数、印刷保真度预测、层粘合检查、基材选择和固化方法,以实现精细的功能复合材料。本研究还重点详细介绍了其在电子、医疗和机械领域的应用。
{"title":"Direct Ink Writing of Carbon-Doped Polymeric Composite Ink: A Review on Its Requirements and Applications.","authors":"Ratnesh Raj, Amit Rai Dixit","doi":"10.1089/3dp.2021.0209","DOIUrl":"10.1089/3dp.2021.0209","url":null,"abstract":"<p><p>Direct Ink Writing (DIW) opens new possibilities in three-dimensional (3D) printing of carbon-based polymeric ink. This is due to its ability in design flexibility, structural complexity, and environmental sustainability. This area requires exhaustive study because of its wide application in different manufacturing sectors. The present article is related to the variant emerging 3D printing techniques and DIW of carbonaceous materials. Carbon-based materials, extensively used for various applications in 3D printing, possess impressive chemical stability, strength, and flexible nanostructure. Fine printable inks consist predominantly of uniform solutions of carbon materials, such as graphene, graphene oxide (GO), carbon fibers (CFs), carbon nanotubes (CNTs), and solvents. It also contains compatible polymers and suitable additives. This review article elaborately discusses the fundamental requirements of DIW in structuring carbon-doped polymeric inks viz. ink formulation, required ink rheology, extrusion parameters, print fidelity prediction, layer bonding examination, substrate selection, and curing method to achieve fine functional composites. A detailed description of its application in the fields of electronics, medical, and mechanical segments have also been focused in this study.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"828-854"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10440670/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10059367","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-01Epub Date: 2023-08-09DOI: 10.1089/3dp.2021.0118
Aboubaker I B Idriss, Jian Li, Yanling Guo, Tong Shuhui, Yangwei Wang, Elkhawad A Elfaki, Gafer A Ahmed
The current available selective laser sintering (SLS) materials are often high in cost and limited in variety; the mechanical properties of wood-composite SLS parts are low quality, which restricts the development of SLS technology. This article aims to optimize the SLS processing parameters to enhance the mechanical properties of the Prosopis chilensis powder (PCP)/polyethersulfone (PES) composite (PCPC) part fabricated via SLS. The PCP and PES powder were proposed as the feedstock of the PCPC powder bed for SLS. First, the thermal decomposition and glass transition temperatures (Tg) of PCP and PES powder were estimated to reduce the produced PCPC parts from warping and deformation during SLS. An orthogonal experimental methodology with five factors and four levels was used to optimize the SLS parameters for the PCPC SLS test. The scanning speed, preheating temperature, and laser power are selected as the main affecting factors on this study. The influence of these factors on dimension accuracies, bending and tensile strengths, and surface roughness quality of the produced PCPC parts was studied. The PCPC particle distribution and microstructure were inspected via scanning electron microscopy. Furthermore, the synthesis weighted scoring methods were utilized to determine the optimal SLS processing parameters of the produced PCPC parts. The combined results of tests showed that the optimal SLS parameters were as follows: the scanning speed is 1.8 m/s, preheating temperature is 80°C, and the laser power is 12 W. Thus, the quality of PCPC SLS parts was significantly enhanced when the optimal parameters were utilized in the SLS process. This article provided the main reference values of SLS parameters of the PCPC. To further enhance the surface roughness quality and mechanical strengths, the postprocessing infiltration with wax was introduced; after wax infiltration, the surface roughness and mechanical strengths were significantly improved.
{"title":"Selective Laser Sintering Parameter Optimization of Prosopis Chilensis/Polyethersulfone Composite Fabricated by AFS-360 SLS.","authors":"Aboubaker I B Idriss, Jian Li, Yanling Guo, Tong Shuhui, Yangwei Wang, Elkhawad A Elfaki, Gafer A Ahmed","doi":"10.1089/3dp.2021.0118","DOIUrl":"10.1089/3dp.2021.0118","url":null,"abstract":"<p><p>The current available selective laser sintering (SLS) materials are often high in cost and limited in variety; the mechanical properties of wood-composite SLS parts are low quality, which restricts the development of SLS technology. This article aims to optimize the SLS processing parameters to enhance the mechanical properties of the Prosopis chilensis powder (PCP)/polyethersulfone (PES) composite (PCPC) part fabricated via SLS. The PCP and PES powder were proposed as the feedstock of the PCPC powder bed for SLS. First, the thermal decomposition and glass transition temperatures (Tg) of PCP and PES powder were estimated to reduce the produced PCPC parts from warping and deformation during SLS. An orthogonal experimental methodology with five factors and four levels was used to optimize the SLS parameters for the PCPC SLS test. The scanning speed, preheating temperature, and laser power are selected as the main affecting factors on this study. The influence of these factors on dimension accuracies, bending and tensile strengths, and surface roughness quality of the produced PCPC parts was studied. The PCPC particle distribution and microstructure were inspected via scanning electron microscopy. Furthermore, the synthesis weighted scoring methods were utilized to determine the optimal SLS processing parameters of the produced PCPC parts. The combined results of tests showed that the optimal SLS parameters were as follows: the scanning speed is 1.8 m/s, preheating temperature is 80°C, and the laser power is 12 W. Thus, the quality of PCPC SLS parts was significantly enhanced when the optimal parameters were utilized in the SLS process. This article provided the main reference values of SLS parameters of the PCPC. To further enhance the surface roughness quality and mechanical strengths, the postprocessing infiltration with wax was introduced; after wax infiltration, the surface roughness and mechanical strengths were significantly improved.</p>","PeriodicalId":54341,"journal":{"name":"3D Printing and Additive Manufacturing","volume":"10 4","pages":"697-710"},"PeriodicalIF":2.3,"publicationDate":"2023-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10440679/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10433422","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}