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Structural and Optical Studies on WO3/SnO2 and WO3/SnO2/SrO Composites WO3/SnO2 和 WO3/SnO2/SrO 复合材料的结构和光学研究
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-10 DOI: 10.1007/s11664-024-11412-2
N. Gopinathan, K. Kamalnathan, S. Sathik Basha, M. Mubeen

Doping is a widely explored technique to modify the properties of semiconducting materials. In the case of tungsten trioxide (WO3), doping with elements such as SnO2 and SrO has garnered significant attention owing to its potential impact on structural, functional, and optical characteristics. We report on structural, functional, optical, and dielectric properties of SnO2/WO3 and SrO/SnO2/WO3 composites and, for comparison, WO3 prepared via a wet chemical method. Crystallite phases were confirmed using x-ray diffraction patterns. Fourier-transform infrared spectroscopy and dielectric studies were employed to analyze the functional groups, dielectric constants, and losses of the SnO2/WO3 and WO3/SnO2/SrO composites. Ultraviolet-visible spectroscopy and photoluminescence spectroscopy were used to examine the optical absorption and emission maxima, respectively. The energy bandgap was determined from the absorption spectra by using a Tauc plot. Additionally, all the prepared composites exhibited brighter and sharper narrow emissions in the photoluminescence spectra. Dielectric studies of WO3/SnO2/SrO composites revealed slightly better dielectric constants and lower dielectric losses than those of SnO2/WO3 composites. Our findings suggest that the prepared composites are suitable for use in sensor and optoelectronic device applications.

掺杂是一种被广泛探索的改变半导体材料特性的技术。就三氧化钨 (WO3) 而言,掺杂 SnO2 和 SrO 等元素因其对结构、功能和光学特性的潜在影响而备受关注。我们报告了 SnO2/WO3 和 SrO/SnO2/WO3 复合材料以及通过湿化学方法制备的 WO3 的结构、功能、光学和介电特性。利用 X 射线衍射图样确认了晶相。傅立叶变换红外光谱和介电研究用于分析 SnO2/WO3 和 WO3/SnO2/SrO 复合材料的官能团、介电常数和损耗。紫外-可见光谱和光致发光光谱分别用于研究光吸收和发射最大值。能带隙是通过陶氏图从吸收光谱中确定的。此外,所有制备的复合材料在光致发光光谱中都表现出更明亮、更锐利的窄发射。对 WO3/SnO2/SrO 复合材料的介电研究表明,其介电常数和介电损耗均略高于 SnO2/WO3 复合材料。我们的研究结果表明,所制备的复合材料适用于传感器和光电设备应用。
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引用次数: 0
Rhizopus Hyphae Carbon as Efficient Sulfur Host For Lithium–Sulfur Batteries 根瘤菌菌丝碳作为锂硫电池的高效硫宿主
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-10 DOI: 10.1007/s11664-024-11403-3
Weiyong Zhang, Long Wang, Lei Huang, Xinping He, Xinqi Liang, Xinhui Xia, Yongqi Zhang, Feng Cao, Minghua Chen, Wangjun Wan, Chen Wang, Yang Xia, Jun Zhang, Wenkui Zhang

Construction of advanced carbon material is critical for the development of high-performance lithium–sulfur batteries. In this work, we report Rhizopus hyphae biomass carbon (RHBC) as a host material for the sulfur cathode of lithium–sulfur batteries. The porous structure of the RHBC is optimized through hydrothermal activation using KOH solution. The introduction of RHBC into the cathode not only enhances the electronic conductivity of the sulfur cathode, but also substantially improves the capacity of the active materials. Additionally, the RHBC can effectively relieve the volume expansion problem of the sulfur conversion reaction and maintain structural stability, leading to improved lifetime and capacity. Accordingly, the KOH-activated RHBC/S cathode presents initial discharge specific capacity of 748 mAh/g at current density of 0.1 C. Furthermore, the porous structure facilitates rapid transport of electrons and ions, thereby enabling good high-rate performance.

先进碳材料的构建对于高性能锂硫电池的开发至关重要。在这项工作中,我们报道了根瘤菌菌丝生物质碳(RHBC)作为锂硫电池硫阴极的宿主材料。通过使用 KOH 溶液进行水热活化,优化了 RHBC 的多孔结构。在阴极中引入 RHBC 不仅能增强硫阴极的电子导电性,还能大幅提高活性材料的容量。此外,RHBC 还能有效缓解硫转化反应的体积膨胀问题,并保持结构的稳定性,从而提高寿命和容量。因此,KOH 激活的 RHBC/S 阴极在电流密度为 0.1 C 时的初始放电比容量为 748 mAh/g。此外,多孔结构有利于电子和离子的快速传输,从而实现了良好的高速性能。
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引用次数: 0
Sr-Yb Co-doping of BaCe0.4Zr0.6O3 Proton-Conducting Electrolyte for Solid Oxide Fuel Cells 用于固体氧化物燃料电池的 BaCe0.4Zr0.6O3 质子传导电解质的 Sr-Yb Co 掺杂
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-10 DOI: 10.1007/s11664-024-11400-6
Jihai Cheng, Lingling Xu, Hao Liang

Ba0.9Sr0.1Ce0.4Zr0.6−xYbxO3−δ(x = 0.05, 0.1, 0.15, 0.2) proton-conducting electrolyte powders were synthesized by the nitrate combustion method. The effects of co-doping of Sr and Yb on the phase composition and electrochemical performance were studied. X-ray diffraction (XRD) results indicate that Sr and Yb were successfully doped into the lattice of BaCe0.4Zr0.6O3, forming a single perovskite phase. The AC impedance technique was used to investigate the total conductivity of the materials under air and water vapor atmospheres at 400–800°C. The results show that BSCZY20 demonstrated the highest electrical conductivity of 0.033 S cm−1 at 800°C in water vapor. This suggests that the co-doping strategy can effectively enhance the conductivity of BaCe0.4Zr0.6O3 proton-conducting material, which provides valuable insight for the development of high-performance proton-conducting solid oxide fuel cells.

采用硝酸盐燃烧法合成了 Ba0.9Sr0.1Ce0.4Zr0.6-xYbxO3-δ(x = 0.05、0.1、0.15、0.2)质子传导电解质粉末。研究了 Sr 和 Yb 共掺杂对相组成和电化学性能的影响。X 射线衍射 (XRD) 结果表明,Sr 和 Yb 成功地掺杂到了 BaCe0.4Zr0.6O3 的晶格中,形成了单一的包晶相。交流阻抗技术用于研究材料在 400-800°C 的空气和水蒸气环境下的总电导率。结果表明,BSCZY20 在 800°C 水蒸气环境下的导电率最高,达到 0.033 S cm-1。这表明共掺杂策略能有效提高 BaCe0.4Zr0.6O3 质子导电材料的电导率,为开发高性能质子传导型固体氧化物燃料电池提供了宝贵的启示。
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引用次数: 0
Effects of Silver Nanoparticles in Pectin Polysaccharide Thin Film on Resistive Switching Characteristics 果胶多糖薄膜中的纳米银粒子对电阻开关特性的影响
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-09 DOI: 10.1007/s11664-024-11401-5
Jia Zheng Yeoh, Muhammad Awais, Feng Zhao, Kuan Yew Cheong

This study investigates the resistive switching characteristics of Ag nanoparticle (AgNP)-incorporated pectin (pectin-AgNP) as a memristive thin film, with varying concentrations of AgNP (0.0 wt.%, 0.5 wt.%, and 1.0 wt.%) and pectin (5.0 mg/L, 5.5 mg/L, 6.0 mg/L, 6.5 mg/L, and 7.0 mg/L), sandwiched between Au and indium tin oxide (ITO) electrodes on glass substrate. The structural, chemical, and electrical properties of these pectin-AgNP thin films were evaluated. With AgNP concentration of 0.5 wt.% in a pectin concentration of 5.5 mg/mL, the Fourier transform infrared (FTIR) spectra indicated the highest presence of C–O bonds. This suggests the incorporation of AgNP and the formation of more linear and extended pectin chains established by glycosidic bonds. The abundance of C–O bonds contributed significantly to the increase in the resistance of the thin film, consequently yielding the highest ON/OFF ratio (7.2 × 103) observed among the samples. The electronic and thermochemical mechanisms governing the resistive switching behaviours were also proposed.

Graphical Abstract

本研究探讨了Ag纳米粒子(AgNP)-包合果胶(果胶-AgNP)作为记忆薄膜的电阻开关特性,不同浓度的AgNP(0.0 wt.%、0.5 wt.% 和 1.0 wt.%)和果胶(5.0 mg/L、5.5 mg/L、6.0 mg/L、6.5 mg/L 和 7.0 mg/L),夹在玻璃基板上的金电极和铟锡氧化物(ITO)电极之间。对这些果胶-AgNP 薄膜的结构、化学和电学特性进行了评估。果胶浓度为 5.5 mg/mL 时,AgNP 的浓度为 0.5 wt.%,傅立叶变换红外光谱(FTIR)显示 C-O 键的存在率最高。这表明 AgNP 的加入以及通过糖苷键形成的果胶链更加线性和延伸。C-O 键的大量存在极大地促进了薄膜电阻的增加,因此在所有样品中产生了最高的导通/关断比(7.2 × 103)。此外,还提出了支配电阻开关行为的电子和热化学机制。
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引用次数: 0
Teeth-Shaped Waveguide-Driven Tunable Band-Stop Plasmonic Filter in the Near-Infrared Region 近红外区域的齿形波导驱动可调谐带挡等离子滤波器
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-09 DOI: 10.1007/s11664-024-11410-4
Ghasem KhosroBeygi, Mohammad Reza Jafari, Mehran Shahmansouri

A tunable plasmonic filter in the near-infrared range is being investigated using the finite element numerical method (FEM). The filter structure consists of a serrated dielectric layer, which includes an air layer and silica teeth sandwiched between two metal layers. A numerical analysis shows that it is possible to adjust the band-stop amplitude, intensity, and band-pass width by changing the geometrical parameters. The proposed structure is expected to be used as an essential component of photonics devices due to its ability to confine light in the sub-wavelength region.

目前正在使用有限元数值法(FEM)研究一种近红外范围的可调谐等离子滤波器。滤波器结构由锯齿状介电层组成,其中包括夹在两层金属之间的空气层和硅齿。数值分析表明,可以通过改变几何参数来调整带挡振幅、强度和带通宽度。由于这种结构能够将光限制在亚波长区域,因此有望成为光子器件的重要组成部分。
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引用次数: 0
Enhanced Piezoelectric Performance in Nickel Oxide Nanoparticle-Embedded Flexible PVDF Film 增强氧化镍纳米粒子嵌入柔性 PVDF 薄膜的压电性能
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-06 DOI: 10.1007/s11664-024-11363-8
Arun Mondal, Mohd Faraz, Neeraj Khare

The conversion of ambient mechanical vibrations into electricity using piezoelectric nanogenerators (PENGs) has garnered significant attention from researchers over the past few years, in light of its potential in wearable applications. The high flexibility and significant ferroelectricity of poly(vinylidene fluoride) (PVDF) make them the most promising candidates for PENG applications among polymer piezoelectric materials. In the present work, NiO nanoparticles were incorporated in different ratios into a PVDF matrix, and their potential for use in piezoelectric nanogenerators was investigated. The PVDF/NiO (5 wt.%) nanocomposite PENG exhibited the highest electrical output, with a 2.8-fold increase in open-circuit voltage and short-circuit current observed as compared to a bare PVDF-based PENG. However, a further increase in the compositional ratio of NiO led to a decrease in PENG output. The improved piezoelectricity in the PVDF/NiO (5 wt.%) nanocomposite is attributed to the enhanced polar phases and improved ferroelectricity of PVDF. Further confirmation of the improved piezoresponse was explored by measurement of the piezoelectric coefficient (d33) and dielectric study of the nanocomposites. The PENG electrical output was further simulated using the finite elemental method in COMSOL Multiphysics 5.5. The simulated results matched well with the experimental output, which confirmed the improved electrical performance of the PVDF/NiO nanocomposite-based PENGs. The enhanced performance of the nanocomposite PVDF film is attributed to the higher β phase in the PVDF. The efficiency of the PENG devices in motion-sensing applications was also explored. Different output voltage signals corresponding to different movements of the nanocomposite-based PENGs make the device compatible with sensor applications.

在过去几年中,利用压电纳米发电机(PENGs)将环境机械振动转化为电能的技术因其在可穿戴应用中的潜力而备受研究人员的关注。聚偏二氟乙烯(PVDF)具有高柔韧性和显著的铁电性,是聚合物压电材料中最有希望应用于压电纳米发电机的材料。本研究将不同比例的氧化镍纳米颗粒加入到 PVDF 基体中,并研究了它们在压电纳米发电机中的应用潜力。与裸 PVDF 基 PENG 相比,PVDF/NiO(5 wt.%)纳米复合材料 PENG 的电输出最高,开路电压和短路电流增加了 2.8 倍。然而,NiO 成分比的进一步增加会导致 PENG 输出下降。PVDF/NiO (5 wt.%)纳米复合材料压电性的改善归因于极性相的增强和 PVDF 铁电性的改善。通过测量压电系数(d33)和对纳米复合材料进行介电研究,进一步证实了压电响应的改善。使用 COMSOL Multiphysics 5.5 中的有限元法进一步模拟了 PENG 的电气输出。模拟结果与实验结果十分吻合,证实了基于 PVDF/NiO 纳米复合材料的 PENG 的电性能得到了改善。纳米复合 PVDF 薄膜性能的提高归功于 PVDF 中较高的β相。此外,还探讨了 PENG 器件在运动感应应用中的效率。与基于纳米复合材料的 PENG 的不同运动相对应的不同输出电压信号使该器件与传感器应用兼容。
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引用次数: 0
Enhancement of Dye Degradation in Piezo-Photocatalytic ZnO–MoS2 Heterostructures 增强压电光催化 ZnO-MoS2 异质结构的染料降解能力
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-06 DOI: 10.1007/s11664-024-11413-1
James Albert B. Narvaez, Candy C. Mercado

Photocatalysis is a novel approach to degrade hazardous compounds, frequently employed in environmental remediation such as eliminating methyl orange (MO) dye from wastewater. However, low efficient usage of visible light due to the large band gap of photocatalysts and its high rate of recombination limit the process. To address this issue, piezophototronics has been utilized to improve the efficacy of catalytic degradation. Specifically for this study, the piezo-photocatalytic efficiency of ZnO–MoS2 heterostructures has been realized using solar and mechanical energy in degrading MO dye. One-dimensional heterostructures with an average length of 3.34 μm and an average diameter of 872.6 nm compactly aligned on glass substrates were synthesized through a two-step hydrothermal process. Under simulated solar illumination and ultrasonic vibration, the ZnO–MoS2 effectively degraded MO, improving the degradation efficiency from 55% to 84% by introducing piezopotential in ZnO. Ultrasonication aided the photocatalysis through field-assisted separation of the photogenerated electrons and holes, reducing recombination. Coupled liquid chromatography and mass spectrometry confirmed the degradation of MO into its smaller metabolites. The catalyst films have achieved 61% degradation even after 3 times reuse.

光催化是一种降解有害化合物的新方法,经常用于环境修复,如消除废水中的甲基橙(MO)染料。然而,由于光催化剂的带隙较大且重组率较高,可见光的使用效率较低,从而限制了光催化过程。为了解决这一问题,人们利用压电光电技术来提高催化降解的效率。本研究利用太阳能和机械能实现了 ZnO-MoS2 异质结构在降解 MO 染料时的压光催化效率。研究人员通过两步水热法合成了平均长度为 3.34 μm、平均直径为 872.6 nm 的一维异质结构,这些异质结构紧密排列在玻璃基底上。在模拟太阳光照射和超声波振动下,ZnO-MoS2 能有效降解 MO,通过在 ZnO 中引入压电势,降解效率从 55% 提高到 84%。超声通过场辅助分离光生电子和空穴,减少了重组,从而有助于光催化。耦合液相色谱法和质谱法证实了 MO 被降解为更小的代谢物。即使重复使用 3 次,催化剂薄膜的降解率也达到了 61%。
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引用次数: 0
Study of the Structure, Microstructure, and Electrical Properties of Defect-Induced Ce-Doped SrTiO3 as Solid Electrolyte in IT-SOFC Application 将缺陷诱导掺杂 Ce 的 SrTiO3 作为 IT-SOFC 应用中的固体电解质的结构、微观结构和电性能研究
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-05 DOI: 10.1007/s11664-024-11392-3
Vedika Yadav, Upendra Kumar

Ionic conductors with the composition SrTi1−xCexO3 (x = 0, 0.02, and 0.04) were synthesized by a high-temperature conventional ceramic route, and their electrical properties were analyzed for use as solid electrolytes in intermediate-temperature solid oxide fuel cells (IT-SOFCs). Scanning electron microscopy/energy-dispersive x-ray spectroscopy (SEM-EDX) was used to analyze the compositional homogeneity and morphology of the samples. The phase analysis was performed using X-ray diffraction (XRD), followed by Rietveld refinement, confirming the cubic crystal structure under the space group (Pmoverline{3 }m). The bands at 462 cm−1 and 449 cm−1 in the Raman spectrum confirmed the incorporation of Ce at the Ti-site of SrTiO3. The presence of a negative charge was found from zeta potential analysis, supporting the presence of Ce3+ at the Ce4+site, denoted by (C{e}_{C{e}^{4+}}^{3+}{^prime}), and Ti3+ at the Ti4+ site, denoted by (T{i}_{T{i}^{4+}}^{3+}{^prime}), in X-ray photoelectron spectroscopy (XPS) analysis. The total conductivity of samples showed thermal-dependent Arrhenius behavior with two different activation energy values. The activation energy (ge 1 text{eV}) in high-temperature regions indicated the migration of doubly ionized oxygen vacancy and (le 0.50 text{eV}) reflecting the migration of electrons between the degenerate sites of Ti4+/Ce4+. The impedance spectroscopy studies suggested the presence of bulk contribution in the electrical properties, and similar charge carriers were responsible for both processes. The impact of oxygen vacancy on electrical conduction was also supported by the magnetic properties, which displayed diamagnetic to paramagnetic phase transition with Ce doping. The highest value of total conductivity was obtained around 0.003 S cm−1 at 610°C, making it a potential candidate for solid electrolytes in IT-SOFC applications.

通过高温传统陶瓷路线合成了 SrTi1-xCexO3 (x = 0、0.02 和 0.04)离子导体,并分析了它们在中温固体氧化物燃料电池(IT-SOFC)中用作固体电解质的电学特性。扫描电子显微镜/能量色散 X 射线光谱法(SEM-EDX)用于分析样品的成分均匀性和形态。利用 X 射线衍射 (XRD) 进行了相分析,然后进行了里特维尔德细化,确认了空间群为立方晶体结构。拉曼光谱中 462 cm-1 和 449 cm-1 处的波段证实了在 SrTiO3 的 Ti 位上掺入了 Ce。在 X 射线光电子能谱(XPS)分析中,ZETA 电位分析发现了负电荷的存在,支持了 Ce4+ 位点上 Ce3+ 的存在,用 (C{e}_{C{e}^{4+}}^{3+}{^prime} 表示;Ti4+ 位点上 Ti3+ 的存在,用 (T{i}_{T{i}^{4+}}^{3+}{^prime} 表示。样品的总电导率表现出两种不同活化能值的热依赖性阿伦尼乌斯行为。高温区的活化能(ge 1 text{eV})表明了双电离氧空位的迁移,而(le 0.50 text{eV})则反映了电子在 Ti4+/Ce4+ 的退化位点之间的迁移。阻抗光谱研究表明,在电学特性中存在块体贡献,而且类似的电荷载流子对这两个过程都负有责任。氧空位对电导的影响也得到了磁性能的支持,在掺杂 Ce 时,磁性能显示出从二磁性到顺磁性的相变。在 610°C 时,总电导率的最高值约为 0.003 S cm-1,使其成为 IT-SOFC 应用中固体电解质的潜在候选材料。
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引用次数: 0
Effect of Annealing Treatment on Electromigration Resistance of Low-Temperature Sn-57Bi-1Ag Solder Interconnect 退火处理对低温锡-57铋-1Ag 焊料互连器件抗电迁移性能的影响
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-05 DOI: 10.1007/s11664-024-11402-4
J. L. Chen, S. B. Wang, J. Ren, M. L. Huang

The effect of annealing treatment on the electromigration (EM) resistance of low-temperature Cu/Sn-57Bi-1Ag (600 μm)/Cu solder interconnects has been investigated. The annealing treatment of as-soldered Cu/Sn-57Bi-1Ag/Cu solder interconnects caused the obvious coarsening of Bi phases in the bulk solders and a slight reduction in the electric resistance of the solder interconnects. The coarsening of the Bi phases induced a decrease in the Bi/β-Sn phase boundaries and thus a decrease in the EM-induced atomic diffusion flux of Bi atoms during the subsequent current stressing, resulting in the segregation of a thinner Bi phase layer at the anode and a lower increase rate of electric resistance of the solder interconnects. The longer the annealing time, the higher the EM resistance of the solder interconnects. The reductions in both the effective diffusion coefficient of the Bi atoms and the electric resistivity of the bulk Sn-57Bi-1Ag solders induced by the annealing treatment were responsible for the higher EM resistance of low-temperature Sn-57Bi-1Ag solder interconnects.

研究了退火处理对低温 Cu/Sn-57Bi-1Ag (600 μm)/Cu 焊料互连器件的电迁移(EM)电阻的影响。对焊接后的 Cu/Sn-57Bi-1Ag/Cu 焊料互连器件进行退火处理后,散装焊料中的 Bi 相明显粗化,焊料互连器件的电阻略有降低。Bi 相的粗化导致 Bi/β-Sn 相界减小,因此在随后的电流应力过程中,电磁诱导的 Bi 原子扩散通量也随之减小,从而在阳极形成较薄的 Bi 相分离层,降低了焊料互连器件的电阻增加率。退火时间越长,焊料互连的电磁电阻越高。退火处理导致 Bi 原子的有效扩散系数和锡-57Bi-1Ag 焊料的电阻率降低,是低温锡-57Bi-1Ag 焊料互连器件的电磁电阻较高的原因。
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引用次数: 0
Synthesis of Graphene/Tungsten Carbide (WC) Nanocomposites from Palm Oil via Pulsed Arc Discharge in Liquid Medium: Morphological, Functional, and Gas Sensing Characterization 在液体介质中通过脉冲电弧放电从棕榈油中合成石墨烯/碳化钨 (WC) 纳米复合材料:形态、功能和气体传感表征
IF 2.1 4区 工程技术 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Pub Date : 2024-09-05 DOI: 10.1007/s11664-024-11371-8
Siti Zubaidah Siddick, Shaifulazuar Rozali, Yew Hoong Wong, Nabilah Mohamad Yusof

With recent trends moving towards sustainable approaches in adherence to environmental, social, and governance (ESG) standards, research is actively focused on sustainable production of high-potential materials. In this study, a successful synthesis pathway was demonstrated for a graphene/tungsten carbide (WC) nanocomposite via pulsed arc discharge in liquid medium, utilizing crude palm oil and commercial cooking palm oil as liquid precursors. The synthesis of the graphene/WC nanocomposites was carried out by applying current with amplitude of 80 A and 100 A to the tungsten electrode immersed in the liquid palm oil, subjected to 150 arc discharges. A comparative investigation was performed to examine the morphological and functional characteristics of the materials synthesized from the different types of palm oil under different current conditions. In addition, the synthesized nanocomposites were assessed with respect to their gas sensing performance. Impressively, the CRG100(150) nanocomposite (produced from crude palm oil with current of 100 A) exhibited gas sensing response of 4.853% upon injection of 200 ppm of ethanol. The CRG100(150) nanocomposite also demonstrated short response and recovery time of 43 s and 182 s, respectively. Thus, the successful synthesis of CRG100(150), utilizing a natural precursor via arc discharge in liquid, paves the way for the development of sustainable gas sensing materials.

随着最近的趋势朝着符合环境、社会和治理(ESG)标准的可持续方法发展,研究人员正积极关注高潜力材料的可持续生产。本研究利用粗棕榈油和商用烹饪棕榈油作为液体前驱体,通过脉冲电弧放电在液体介质中成功合成了石墨烯/碳化钨(WC)纳米复合材料。合成石墨烯/碳化钨纳米复合材料的方法是向浸入液态棕榈油中的钨电极施加振幅分别为 80 A 和 100 A 的电流,并进行 150 次电弧放电。在不同的电流条件下,对不同类型的棕榈油合成材料的形态和功能特性进行了比较研究。此外,还对合成的纳米复合材料的气体传感性能进行了评估。令人印象深刻的是,CRG100(150)纳米复合材料(由粗棕榈油制成,电流为 100 A)在注入 200 ppm 乙醇时的气体传感响应为 4.853%。CRG100(150) 纳米复合材料的响应时间和恢复时间也很短,分别为 43 秒和 182 秒。因此,利用天然前驱体在液体中通过电弧放电成功合成 CRG100(150),为开发可持续气体传感材料铺平了道路。
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Journal of Electronic Materials
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