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Size scaling of printed microstructures using a lift-off printing (LoP) process 采用升降式印刷(LoP)工艺的微结构印刷尺寸缩放
Yu-Min Fu, Y. Liang, Y. T. Cheng, Pu-Wei Wu
Inkjet printing has been one of fascinating techniques for microfabrication owing to the characteristics of low manufacturing cost, low processing temperature, low material usage,...etc. [1, 2]. In this work, a Lift-off Printing (LoP) process combining conventional photolithography and inkjet printing processes is introduced to realize printed size-scalable silver microstructures with the line width of 5 up to 70 μm and the resistivity of ~5.7 μΩ · cm on a silicon substrate. In addition, an as-printed interdigitated capacitor with the electrode size and spacing of 10μm has been successfully demonstrated with a capacitance of 2.3 pF/mm2@10kHz.
喷墨打印具有制造成本低、加工温度低、材料用量少等特点,已成为微加工领域的热门技术之一。[1,2]。本文介绍了一种结合传统光刻和喷墨印刷工艺的起升式印刷(LoP)工艺,在硅衬底上实现了线宽为5 ~ 70 μm、电阻率为~5.7 μΩ·cm的可缩放银微结构的印刷。此外,还成功印制了电极尺寸和间距为10μm、电容为2.3 pF/mm2@10kHz的双指电容。
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引用次数: 0
Fabrication of spiral-shaped PVDF cantilever based vibration energy harvester 螺旋型PVDF悬臂振动能量采集器的研制
Wen Liu, Mengdi Han, Xuming Sun, Haixia Zhang
Polyvinylidene fluoride (PVDF) has a strong piezoelectricity. With the piezoelectric coefficient of poled thin films as large as 6-7 pC/N, PVDF is becoming a popular material for the sensors and energy harvesting. However, the fabrication process of PVDF is a big challenge due to the physical and chemical properties of PVDF. In this paper, a spiral-shaped PVDF cantilever is fabricated to harvest vibration energy in the environment. Copper mass and silicon mass are added to the PVDF cantilever to reduce the resonant frequency. Series of MEMS fabrication process are utilized to realize the PVDF piezoelectric energy harvester.
聚偏氟乙烯(PVDF)具有很强的压电性。PVDF极化薄膜的压电系数高达6-7 pC/N,正成为传感器和能量收集的热门材料。然而,由于PVDF的物理和化学性质,其制造工艺是一个很大的挑战。本文制作了一种螺旋形PVDF悬臂梁,用于收集环境中的振动能量。在PVDF悬臂梁中加入铜质量和硅质量以降低谐振频率。利用一系列MEMS制造工艺实现了PVDF压电能量采集器。
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引用次数: 3
Co-axially electrospun PVDF fibers with hollow wall to enhance potential output 同轴静电纺丝聚偏氟乙烯纤维与空心壁,以提高电位输出
Y. Lai, H. Wu, C. Pan, C. Yen, C. Tsao, Liwei Lin, S. Kuo, Y. S. Lu, S. Shen
In this study, a CNFES (cylindrical near-field electrospinning) process and a metallic coaxial needle injector were used to fabricate piezoelectric PVDF (polyvinylidene fluoride) hollow-walled fibers. Piezoelectric fibers devices with interdigitated electrode were fabricated to capture potential signal. First, the PVDF powder was mixed in the acetone solution and the fluorosurfactant was dissolved with the dimethyl sulfoxide to prepare PVDF macromolecular solution. Second, PVDF macromolecular solution was filled in the outer needle, air was filled in the syringe of inner needle and the metal needle coaxial injector contacted a high power supply. When the PVDF droplet in the coaxial needle was subjected to high electric field, the droplet overcame surface tension of the solution and became a Taylor cone, extremely fine hollow-walled PVDF fibers was spun out on collectors. The hollow-walled PVDF fibers were collected by a cylindrical device on the XY-axis digital platform. The diameter of hollow-walled PVDF fibers could be controlled by adjusting the electric field and the rotating speed of the cylindrical collector. The experimental images reveal structures of the hollow-walled PVDF fibers. In comparison of the solid PVDF and the hollow-walled PVDF fibers, the solid PVDF fibers with IDT (interdigitated electrode) could generate maximum peak voltage of 35.731-213.827 mV at frequencies of 2-9 Hz, whereas the hollow-walled PVDF fibers with IDT electrode could generate maximum peak voltage of 44.092-246.088 mV. The hollow-walled fibers with higher area/volume ratio and mechanical stiffness can produce more potential voltage.
采用圆柱近场静电纺丝(CNFES)工艺和金属同轴针进样器制备了PVDF(聚偏氟乙烯)压电中空纤维。制作了具有交叉指状电极的压电纤维器件,用于捕获电位信号。首先,将PVDF粉末混合在丙酮溶液中,将含氟表面活性剂与二甲亚砜溶解,制备PVDF大分子溶液。其次,在外针内填充PVDF大分子溶液,在内针注射器内填充空气,金属针同轴注射器与高电源接触。当同轴针中的PVDF液滴受到高电场作用时,液滴克服溶液的表面张力,形成泰勒锥,在集电极上纺出极细的中空PVDF纤维。在xy轴数字平台上采用圆柱形装置采集中空PVDF纤维。通过调节圆柱形集热器的电场和转速,可以控制中空聚乙烯醇纤维的直径。实验图像显示了中空PVDF纤维的结构。对比固体PVDF和空心PVDF光纤,在2 ~ 9 Hz频率下,采用IDT电极的固体PVDF光纤可产生35.731 ~ 213.827 mV的峰值电压,而采用IDT电极的空心PVDF光纤可产生44.092 ~ 246.088 mV的峰值电压。具有较高的面积体积比和机械刚度的空心壁纤维可以产生更高的电位。
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引用次数: 0
Microfabrication of high aspect ratio microtube arrays to store high density charged particles 存储高密度带电粒子的高纵横比微管阵列的微型化
A. Narimannezhad, J. Jennings, M. Weber, K. Lynn
Fabrication of a portable high-density charged particle trap with an array of micro-Penning-Malmberg traps (microtraps) with substantially lower end barrier potentials than conventional Penning-Malmberg traps is presented [1]. The microtraps are designed for antimatter storage such as positrons. The fabrication of large length to radius aspect ratio (1000:1) microtrap arrays involved advanced techniques including photolithography, deep reactive ion etching (DRIE) of silicon wafers to achieve through-vias, gold sputtering of the wafers surfaces and inside the vias, and thermal compression bonding. The bonded stacks were gold electroplated to achieve a uniform gold surface to minimize the patch effects. Positron losses occur in experimentation by trap imperfections such as misalignment of microtraps, asymmetries, and physical imperfections on the surfaces. This paper describes the fabrication issues encountered and addresses geometry errors and asymmetries.
本文提出了一种便携式高密度带电粒子阱的制造方法,该阱具有比传统的Penning-Malmberg阱低得多的端势垒势的微阱阵列[1]。微阱是为储存反物质如正电子而设计的。大长度与半径宽高比(1000:1)微阱阵列的制造涉及先进的技术,包括光刻、硅晶圆的深度反应离子蚀刻(DRIE)以实现通孔、晶圆表面和通孔内部的金溅射以及热压缩键合。结合的堆栈是镀金电镀,以实现一个均匀的金表面,以尽量减少贴片效应。正电子损失发生在实验中的陷阱缺陷,如微陷阱的不对准,不对称和表面的物理缺陷。本文描述了所遇到的制造问题,并解决了几何误差和不对称。
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引用次数: 2
Plasmonic properties of metal nanodot arrays with same diameter utilizing nanoporous alumina mask 利用纳米多孔氧化铝掩膜制备相同直径金属纳米点阵列的等离子体特性
M. Jung, Chulki Kim, Taikjin Lee, J. H. Kim, Seok Lee, Deok-Ha Woo
Metal nanodot arrays with the uniform diameter were fabricated utilizing nanoporous alumina mask with through-holes as an evaporation mask. Ag, Cu, and Au nanodot arrays were fabricated on indium tin oxide coated glass as a replica of the nanoporous alumina mask. The localized surface plasmon resonance (LSPR) properties of metal nanodot arrays were experimentally measured by the ultraviolet-visible spectroscopy. The dependency of LSPR wavelength on nanodot composition was examined.
采用纳米孔氧化铝掩膜作为蒸发掩膜,制备了直径均匀的金属纳米点阵列。在氧化铟锡涂层玻璃上制备了银、铜和金纳米点阵列,作为纳米多孔氧化铝掩膜的复制品。用紫外-可见光谱法测量了金属纳米点阵列的局部表面等离子体共振特性。研究了LSPR波长与纳米点组成的关系。
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引用次数: 0
Focus ion beam based nanofluidic system for biomolecule characterization 基于聚焦离子束的纳米流体系统用于生物分子表征
Taylor Busch, Bo Ma, S. Tung
A Pyrex nanochannel system with embedded transverse nanoelectrodes was designed and fabricated by MEMS based microfabrication and focused ion beam (FIB) nanolithography. The microchannels and microelectrodes in the system were patterned on a Cr/Au coated Pyrex wafer using conventional photolithography while the nanoelectrodes (100 nm wide and 50 nm thick) and the nanochannels (500 nm to 1 μm wide and 100 nm deep) were fabricated by FIB nanolithography. A Pyrex chip coated with amorphous silicon was used as the capping piece to seal off the nanochannels and nanoelectrodes through anodic bonding. Fluorescein isothiocyanate (FITC) solution was pumped through the completed nanochannel system after wetting steps to verify flow patency. The electrical conductivity of four different liquids solutions were measured in the nanochannel system and compared to their bulk values. Translocation of negatively charged nanobeads with an average diameter of 20 nm was successfully carried out and the instantaneous transverse electrical conductivity of the translocating nanobeads was measured by the embedded nanoelectrodes.
采用基于MEMS的微加工和聚焦离子束纳米光刻技术,设计并制备了一种嵌入横向纳米电极的Pyrex纳米通道系统。微通道和微电极采用传统光刻技术在Cr/Au涂层的Pyrex晶圆上进行了设计,纳米电极(100 nm宽,50 nm厚)和纳米通道(500 nm ~ 1 μm宽,100 nm深)采用FIB纳米光刻技术制备。采用包覆非晶硅的耐热玻璃芯片作为封盖片,通过阳极键合将纳米通道和纳米电极封闭。在润湿步骤后,将异硫氰酸荧光素(FITC)溶液泵入完成的纳米通道系统以验证流动通畅性。在纳米通道系统中测量了四种不同液体溶液的电导率,并与它们的体积值进行了比较。成功地实现了平均直径为20 nm的带负电荷纳米珠的易位,并通过嵌入的纳米电极测量了易位后纳米珠的瞬时横向电导率。
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引用次数: 0
First adhesion measurements of conductive ultrananocrystalline diamond MEMS sidewalls 首次测量导电超晶金刚石MEMS侧壁的附着力
F. Buja, J. Kokorian, A. Sumant, W. V. Spengen
We present the first measuremenst of adhesion between two micro-electromechanical systems (MEMS) surfaces, fully fabricated with boron doped ultrananocrystalline diamond (B-UNCD). This research allows us to explore the potential of conductive UNCD MEMS for the solution of issues like adhesion and friction in micro-devices and describe with accuracy the effects involved. By means of standard lithographic techniques, we have fabricated a diamond micro thermal actuator (chevron type), which is used as a platform for tribological testing. A peculiar effect has been observed in the adhesion phenomenon of UNCD. It involves with high probability, an interaction between hydrocarbon/amorphous carbon layers (a-C) that cover the two diamond contacting surfaces. The as-etched device shows a `chewing-gum' effect in the adhesion curve, probably due to the formation of hydrocarbon/a-C chains after the interaction of the surfaces. This effect disappears when the device is treated in oxygen plasma and the hydrocarbon/a-C is removed. The study of this phenomenon will be followed by more accurate analysis and atomistic simulation and the results will be compared with nitrogen-incorporated UNCD (N-UNCD) fabricated devices.
我们提出了两个微机电系统(MEMS)表面之间粘附的第一个测量,完全由硼掺杂超晶金刚石(B-UNCD)制造。这项研究使我们能够探索导电UNCD MEMS在解决微器件中粘附和摩擦等问题方面的潜力,并准确描述所涉及的影响。通过标准的光刻技术,我们制作了一个金刚石微热致动器(v型),作为摩擦学测试的平台。在UNCD的附着现象中观察到一种特殊的效应。它很可能涉及覆盖两个金刚石接触面的碳氢化合物/非晶碳层(a-C)之间的相互作用。蚀刻后的器件在粘附曲线上显示出“口香糖”效应,这可能是由于表面相互作用后形成的碳氢化合物/a- c链。当设备在氧等离子体中处理并去除碳氢化合物/a-C时,这种效应消失。对这一现象的研究将进行更精确的分析和原子模拟,并将结果与氮掺杂UNCD (N-UNCD)制造的器件进行比较。
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引用次数: 1
Fabrication of piezoelectric zinc oxide nanorods by Electrospraying method 电喷涂法制备压电氧化锌纳米棒
Shao-Yu Wang, K. Hung, Y. C. Chen, C. Pan, C. Yen, W. C. Wang, Zong-Hsin Liu
This study mainly used Electrospraying and Taguchi method to investigate the optimum process of piezoelectric Zinc oxide (ZnO) nanorods parameters. Zinc oxide seed layer was electrosprayed on Au/Chromium/Silicon substrates. The electric field is around 660 V/mm. In this study, ZnO was made in an array to characterize. We used X-ray diffraction (XRD), photoluminescence (PL) and field emission scanning electron microscopy (FE-SEM) to characterize the morphology and luminescence of ZnO nanorods. The result showed that with higher and longer of annealing temperature and time. Furthermore, this study was obtained optimum height at 3~5 um of piezoelectric Zinc Oxide nanorods by adopting the process of hydrothermal for 14 hours and with 90 degrees Celsius.
本研究主要采用电喷涂和田口法研究压电氧化锌纳米棒的最佳工艺参数。在Au/铬/硅基底上电喷涂氧化锌种子层。电场≤660v /mm。在本研究中,ZnO被制成阵列来表征。利用x射线衍射(XRD)、光致发光(PL)和场发射扫描电镜(FE-SEM)对ZnO纳米棒的形貌和发光特性进行了表征。结果表明,退火温度越高,退火时间越长。此外,本研究采用90℃的水热工艺,在14小时内获得了3~5 um的压电氧化锌纳米棒的最佳高度。
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引用次数: 0
A micro resonant acceleration sensor comprising silicon support with temperature isolator and quartz doubled ended tuning fork 一种微谐振加速度传感器,包括硅支架与温度隔离器和石英双端音叉
Cun Li, Yulong Zhao, Rongjun Cheng
We present a micro resonant acceleration sensor based on the frequency shift of quartz double ended tuning fork (DETF). The two stiff ends of DETF are mounted on proof mass and temperature isolator structure of silicon support, respectively. Electrodes are coated on the four surfaces of the resonant beam to excite anti-phase vibration model to balance inner stress and torque. Stress in DETF beam shifts when the proof mass is applied to acceleration, which changes resonance frequency of DETF. The temperature isolator structure is designed to reduce the impact of thermal stress due to the difference of thermal expansion coefficient between quartz and silicon. The silicon support and DETF are fabricated based on the bulk micromachining technology. Self-excited circuit is also designed to excite DETF. The proposed sensor is simply packaged for measurement. The sensor takes advantages of both quartz and silicon materials to achieve a micro resonant sensor with simple processing for digital acceleration measurements.
提出了一种基于石英双端音叉频移的微谐振加速度传感器。DETF的两个刚性端分别安装在硅支架的防质量和温度隔离结构上。在谐振梁的四个表面涂覆电极,激发反相位振动模型以平衡内部应力和扭矩。当证明质量作用于加速度时,DETF梁中的应力会发生位移,从而改变DETF的共振频率。为了减小石英与硅的热膨胀系数差异对热应力的影响,设计了隔温器结构。基于本体微加工技术制备了硅支架和DETF。还设计了自激电路来激发DETF。所提出的传感器被简单地封装用于测量。该传感器利用石英和硅材料的优势,实现了一个简单处理的微型谐振传感器,用于数字加速度测量。
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引用次数: 3
Capacitive micromachined ultrasonic transducer for ultra-low pressure detection 用于超低压力检测的电容式微机械超声换能器
Zhikang Li, Libo Zhao, Zhuangde Jiang, Zhiying Ye, Yulong Zhao
This paper presents a novel approach for ultra-low pressure detection using a capacitive micromachined ultrasonic transducer (CMUT) as the sensing element. The working principle depends on the resonant frequency shift of the CMUT under the measured pressure. The finite element method (FEM) simulations were employed to study the sensing performance of the CMUT. The results demonstrated the feasibility and superiority of the CMUT for ultra-low pressure measurement. The resonant frequency varies linearly with the measured pressure. The pressure sensitivity can be improved by increasing the bias DC voltage for a certain CMUT. Additionally, the effects of structure parameters such as electrode dimension, electrode separation distance, membrane radius and thickness on the pressure sensitivity were also studied, which will contribute to the design and operation of the CMUT-based ultra-low pressure sensor.
提出了一种利用电容式微机械超声换能器(CMUT)作为传感元件进行超低压力检测的新方法。其工作原理取决于CMUT在被测压力下的谐振频移。采用有限元方法对CMUT的传感性能进行了仿真研究。结果证明了CMUT用于超低压力测量的可行性和优越性。谐振频率随测量压力呈线性变化。提高某一CMUT的偏置直流电压可以提高压力灵敏度。此外,还研究了电极尺寸、电极分离距离、膜半径和厚度等结构参数对压力灵敏度的影响,为基于cmu的超低压力传感器的设计和运行提供理论依据。
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引用次数: 3
期刊
The 9th IEEE International Conference on Nano/Micro Engineered and Molecular Systems (NEMS)
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